Journal Article PUBDB-2023-07987

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MiniMelt: An instrument for real-time tracking of electron beam additive manufacturing using synchrotron x-ray techniques

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2023
American Institute of Physics [Erscheinungsort nicht ermittelbar]

Review of scientific instruments 94(12), 125103 () [10.1063/5.0177255]
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Abstract: The development of a sample environment for in situ x-ray characterization during metal Electron Beam Powder Bed Fusion (PBF-EB), called MiniMelt, is presented. The design considerations, the features of the equipment, and its implementation at the synchrotron facility PETRA III at Deutsches Elektronen-Synchrotron, Hamburg, Germany, are described. The equipment is based on the commercially available Freemelt ONE PBF-EB system but has been customized with a unique process chamber to enable real-time synchrotron measurements during the additive manufacturing process. Furthermore, a new unconfined powder bed design to replicate the conditions of the full-scale PBF-EB process is introduced. The first radiography (15 kHz) and diffraction (1 kHz) measurements of PBF-EB with a hot-work tool steel and a Ni-base superalloy, as well as bulk metal melting with the CMSX-4 alloy, using the sample environment are presented. MiniMelt enables time-resolved investigations of the dynamic phenomena taking place during multi-layer PBF-EB, facilitating process understanding and development of advanced process strategies and materials for PBF-EB.

Classification:

Contributing Institute(s):
  1. DOOR-User (DOOR ; HAS-User)
  2. Helmholtz-Zentrum Hereon (Hereon)
  3. Experimentebetreuung PETRA III (FS-PET-D)
Research Program(s):
  1. 632 - Materials – Quantum, Complex and Functional Materials (POF4-632) (POF4-632)
  2. 6G3 - PETRA III (DESY) (POF4-6G3) (POF4-6G3)
  3. FS-Proposal: II-20220735 EC (II-20220735-EC) (II-20220735-EC)
  4. FS-Proposal: I-20220349 EC (I-20220349-EC) (I-20220349-EC)
  5. SWEDEN-DESY - SWEDEN-DESY Collaboration (2020_Join2-SWEDEN-DESY) (2020_Join2-SWEDEN-DESY)
Experiment(s):
  1. PETRA Beamline P61.1 (PETRA III)
  2. PETRA Beamline P21.2 (PETRA III)

Appears in the scientific report 2023
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Medline ; Creative Commons Attribution CC BY 4.0 ; OpenAccess ; Clarivate Analytics Master Journal List ; Current Contents - Engineering, Computing and Technology ; Current Contents - Physical, Chemical and Earth Sciences ; Ebsco Academic Search ; Essential Science Indicators ; IF < 5 ; JCR ; National-Konsortium ; PubMed Central ; SCOPUS ; Science Citation Index Expanded ; Web of Science Core Collection
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Private Collections > >Extern > >HAS-User > HAS-User
Private Collections > >DESY > >FS > FS-PET-D
Document types > Articles > Journal Article
Private Collections > >Hereon > Hereon
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 Record created 2023-12-19, last modified 2025-07-24


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