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Journal Article | PUBDB-2017-02115 |
; ; ; ; ;
2016
American Institute of Physics
[S.l.]
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Please use a persistent id in citations: doi:10.1063/1.4967239 doi:10.3204/PUBDB-2017-02115
Abstract: A new method for fast x-ray reflectivity data acquisition is presented. The method is based on a fast rotating, slightly tilted sample reflecting to a stationary mounted position sensitive detector and it allows for measurements of reflectivity curves in a quarter of a second. The resolution in q-space mainly depends on the beam properties and the pixel size of the detector. Maximum q$_{z}$-value of 1 Å$^{−1}$ can be achieved. The time-temperature depending structure changes of poly($N$-isopropylacrylamide) thin films were investigated in situ by applying the fast-reflectivity setup. The results are presented in this paper as illustration of the method and proof of principle.
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