Journal Article

PUBDB-2019-05165

http://join2-wiki.gsi.de/foswiki/pub/Main/Artwork/join2_logo100x88.png Real-Time in Situ Monitoring of Particle and Structure Evolution in the Mechanochemical Synthesis of UiO-66 Metal–Organic Frameworks

Germann, L. S. (Corresponding author) ; Katsenis, A. D. ; Huskić, I. ; Julien, P. A.Extern* ; Užarević, K. ; Etter, M.DESY* ; Farha, O. K. ; Friscic, T. (Corresponding author)Extern* ; Dinnebier, R. E. (Corresponding author)Extern*

2019
ACS Publ. Washington, DC

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Please use a persistent id in citations: doi:10.1021/acs.cgd.9b01477  doi:10.3204/PUBDB-2019-05165

Abstract: While in situ synchrotron X-ray powder diffraction has revolutionized mechanistic studies of mechanochemistry and inspired the development of other real-time monitoring approaches, the full potential of such data remains unexploited, with most applications addressing only reaction kinetics. Focusing on UiO-type metal–organic frameworks (MOFs) as models, we now show how in-depth analysis of real-time diffraction data can provide insight into the evolution of both crystallographic structure and crystallite size, including the direct relation to the particle size of mechanochemically formed MOFs.

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Contributing Institute(s):

1. DOOR-User (DOOR ; HAS-User)
2. Experimentebetreuung PETRA III (FS-PET-D)

Research Program(s):

1. 6213 - Materials and Processes for Energy and Transport Technologies (POF3-621) (POF3-621)
2. 6G3 - PETRA III (POF3-622) (POF3-622)
3. FS-Proposal: I-20150196 (I-20150196) (I-20150196)

Experiment(s):

1. PETRA Beamline P02.1 (PETRA III)

Appears in the scientific report 2019

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Database coverage:
; ; ; Clarivate Analytics Master Journal List ; Current Contents - Physical, Chemical and Earth Sciences ; Ebsco Academic Search ; IF < 5 ; JCR ; NCBI Molecular Biology Database ; SCOPUS ; Science Citation Index ; Science Citation Index Expanded ; Web of Science Core Collection

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