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@ARTICLE{Germann:429645,
author = {Germann, Luzia S. and Katsenis, Athanassios D. and Huskić,
Igor and Julien, Patrick A. and Užarević, Krunoslav and
Etter, Martin and Farha, Omar K. and Friscic, Tomislav and
Dinnebier, Robert E.},
title = {{R}eal-{T}ime in {S}itu {M}onitoring of {P}article and
{S}tructure {E}volution in the {M}echanochemical {S}ynthesis
of {U}i{O}-66 {M}etal–{O}rganic {F}rameworks},
journal = {Crystal growth $\&$ design},
volume = {20},
number = {1},
issn = {1528-7505},
address = {Washington, DC},
publisher = {ACS Publ.},
reportid = {PUBDB-2019-05165},
pages = {49-54},
year = {2019},
abstract = {While in situ synchrotron X-ray powder diffraction has
revolutionized mechanistic studies of mechanochemistry and
inspired the development of other real-time monitoring
approaches, the full potential of such data remains
unexploited, with most applications addressing only reaction
kinetics. Focusing on UiO-type metal–organic frameworks
(MOFs) as models, we now show how in-depth analysis of
real-time diffraction data can provide insight into the
evolution of both crystallographic structure and crystallite
size, including the direct relation to the particle size of
mechanochemically formed MOFs.},
cin = {DOOR ; HAS-User / FS-PET-D},
ddc = {540},
cid = {I:(DE-H253)HAS-User-20120731 /
I:(DE-H253)FS-PET-D-20190712},
pnm = {6213 - Materials and Processes for Energy and Transport
Technologies (POF3-621) / 6G3 - PETRA III (POF3-622) /
FS-Proposal: I-20150196 (I-20150196)},
pid = {G:(DE-HGF)POF3-6213 / G:(DE-HGF)POF3-6G3 /
G:(DE-H253)I-20150196},
experiment = {EXP:(DE-H253)P-P02.1-20150101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000506088200010},
doi = {10.1021/acs.cgd.9b01477},
url = {https://bib-pubdb1.desy.de/record/429645},
}