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000429645 1001_ $$aGermann, Luzia S.$$b0$$eCorresponding author
000429645 245__ $$aReal-Time in Situ Monitoring of Particle and Structure Evolution in the Mechanochemical Synthesis of UiO-66 Metal–Organic Frameworks
000429645 260__ $$aWashington, DC$$bACS Publ.$$c2019
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000429645 520__ $$aWhile in situ synchrotron X-ray powder diffraction has revolutionized mechanistic studies of mechanochemistry and inspired the development of other real-time monitoring approaches, the full potential of such data remains unexploited, with most applications addressing only reaction kinetics. Focusing on UiO-type metal–organic frameworks (MOFs) as models, we now show how in-depth analysis of real-time diffraction data can provide insight into the evolution of both crystallographic structure and crystallite size, including the direct relation to the particle size of mechanochemically formed MOFs.
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000429645 7001_ $$aKatsenis, Athanassios D.$$b1
000429645 7001_ $$aHuskić, Igor$$b2
000429645 7001_ $$0P:(DE-H253)PIP1026734$$aJulien, Patrick A.$$b3
000429645 7001_ $$aUžarević, Krunoslav$$b4
000429645 7001_ $$0P:(DE-H253)PIP1018552$$aEtter, Martin$$b5
000429645 7001_ $$00000-0002-9904-9845$$aFarha, Omar K.$$b6
000429645 7001_ $$0P:(DE-H253)PIP1026729$$aFriscic, Tomislav$$b7$$eCorresponding author
000429645 7001_ $$0P:(DE-H253)PIP1018079$$aDinnebier, Robert E.$$b8$$eCorresponding author
000429645 770__ $$aCrystalline Molecular Materials: FromStructure to Function
000429645 773__ $$0PERI:(DE-600)2048329-6$$a10.1021/acs.cgd.9b01477$$gp. acs.cgd.9b01477$$n1$$p49-54$$tCrystal growth & design$$v20$$x1528-7505$$y2019
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