Journal Article

PUBDB-2019-03098

http://join2-wiki.gsi.de/foswiki/pub/Main/Artwork/join2_logo100x88.png 1 kHz fixed-target serial crystallography using a multilayer monochromator and an integrating pixel detector

Tolstikova, A. (Corresponding author)CFEL*DESY* ; Levantino, M. ; Yefanov, O.CFEL*EMBL*DESY* ; Hennicke, V.CFEL*DESY* ; Fischer, P.CFEL*DESY* ; Meyer, J.DESY* ; Mozzanica, A. ; Redford, S. ; Crosas, E.EMBL*DESY* ; Opara, N. L. ; Barthelmess, M.CFEL*DESY* ; Lieske, J.CFEL*EMBL*DESY* ; Oberthür, D.CFEL*DESY* ; Wator, E. ; Mohacsi, I.CFEL*XFEL.EU* ; Wulff, M.Extern*XFEL.EU* ; Schmitt, B.Extern* ; Chapman, H. N.CFEL*DESY* ; Meents, A. (Corresponding author)CFEL*DESY*

2019
Chester

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Please use a persistent id in citations: doi:10.1107/S205225251900914X  doi:10.3204/PUBDB-2019-03098

Abstract: Reliable sample delivery and efficient use of limited beam time have remained bottlenecks for serial crystallography (SX). Using a high-intensity polychromatic X-ray beam in combination with a newly developed charge-integrating JUNGFRAU detector, we have applied the method of fixed-target SX to collect data at a rate of 1 kHz at a synchrotron-radiation facility. According to our data analysis for the given experimental conditions, only about 3 000 diffraction patterns are required for a high-quality diffraction dataset. With indexing rates of up to 25%, recording of such a dataset takes less than 30 s.

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Contributing Institute(s):

1. FS-CFEL-1 (Group Leader: Henry Chapman) (CFEL-I)
2. CFEL-Coherent X-Ray Imaging (FS-CFEL-1)
3. Experimentebetreuung PETRA III früher FS-PE (FS-PET-D)

Research Program(s):

1. 6215 - Soft Matter, Health and Life Sciences (POF3-621) (POF3-621)
2. X-probe - Advanced XFEL and Synchrotron based Probes of Protein Structure and Dynamics (637295) (637295)
3. EUCALL - European Cluster of Advanced Laser Light Sources (654220) (654220)
4. AXSIS - Frontiers in Attosecond X-ray Science: Imaging and Spectroscopy (609920) (609920)

Experiment(s):

1. Experiments at CFEL
2. Measurement at external facility

Appears in the scientific report 2019

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Database coverage:
; ; ; ; Clarivate Analytics Master Journal List ; Current Contents - Physical, Chemical and Earth Sciences ; DOAJ Seal ; IF >= 5 ; JCR ; NCBI Molecular Biology Database ; PubMed Central ; SCOPUS ; Science Citation Index Expanded ; Web of Science Core Collection

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