Journal Article PUBDB-2026-02288

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Hardening by annealing in the medium-entropy alloy CrCoNi after equal-channel angular pressing

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2026
Elsevier Amsterdam [u.a.]

Materials today / Communications 51, 114751 () [10.1016/j.mtcomm.2026.114751]
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Abstract: After equal-channel angular pressing (ECAP) and a subsequent heat treatment at 600 ◦C for 1 h, the MEA CrCoNiis characterized by a yield strength of about 1.4 GPa but a drastically low uniform elongation of 1.2 %. HighenergyX-ray diffraction analysis, transmission electron microscopy, and high-resolution high-angle annulardark-field scanning transmission electron microscopy investigations were performed, but the cause of theannealing-induced hardening could not be conclusively determined, although differential scanning calorimetrymeasurements reveal an exothermic peak and thus microstructural changes in the temperature range between450 ◦C and 650 ◦C. Despite the complex nature of the MEA CrCoNi, the dominant deformation mechanisms afterECAP processing and a subsequent heat treatment during straining appear to be similar to those of conventionalalloys. It is assumed that the rearrangement of dislocations in low-energy configurations and, to some extent,grain and twin boundary relaxation lead to the anneal-induced hardening effect at 600 ◦C. Grain boundarydislocations are hindered from bowing out or activating new dislocation sources, resulting in the strong increasein yield and ultimate tensile strength.

Classification:

Contributing Institute(s):
  1. DOOR-User (DOOR ; HAS-User)
  2. Helmholtz-Zentrum Hereon (Hereon)
Research Program(s):
  1. 6G3 - PETRA III (DESY) (POF4-6G3) (POF4-6G3)
  2. FS-Proposal: I-20230881 (I-20230881) (I-20230881)
  3. DFG project G:(GEPRIS)468469638 - Einfluss von Zwillingseffekten und Korngrößenverteilung auf das Rissausbreitungsverhalten der Medium-Entropie-Legierung CrCoNi durch hochgradig plastische Verformung und Wärmebehandlung (468469638) (468469638)
Experiment(s):
  1. PETRA Beamline P07 (PETRA III)

Appears in the scientific report 2026
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 Record created 2026-07-30, last modified 2026-07-30


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