Journal Article/Contribution to a conference proceedings PUBDB-2025-01829

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Sample cell for in-situ measurements of ferroelectric polarization and diffraction at beamline P24, DESY

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2025
IOP Publ. Bristol

15th International Conference on Synchrotron Radiation Instrumentation, SRI 2024, HamburgHamburg, Germany, 26 Aug 2024 - 30 Aug 20242024-08-262024-08-30 Journal of physics / Conference Series 3010, 012154 () [10.1088/1742-6596/3010/1/012154]
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Abstract: In-situ measurements of ferroelectric polarization and diffraction under an applied electric field are critical for establishing accurate structure-property correlation. This method captures the dynamic response of ferroelectric materials. To address the challenge of measuring ferroelectric polarization and diffraction data, an in-situ cell equipped with the necessary electronics is developed at the P24 chemical crystallography beamline. Designed sample cell is suitable for measuring ferroelectric polarization and synchrotron X-ray diffraction under an applied electric field for plate shaped crystals. To have temperature control, cartridge heater, peltier element and heat sink are installed and one can perform the experiments in the temperature range of 240K to 420K. The sample cell has been tested with single crystals of KTa0.67Nb0.33NO3(KTN), K0.95Li0.05Ta0.73Nb0.27NO3(Li doped KTN) and BaTiO3(BTO).

Classification:

Note: 2025 J. Phys.: Conf. Ser. 3030

Contributing Institute(s):
  1. PETRA-D (FS-PETRA-D)
Research Program(s):
  1. 631 - Matter – Dynamics, Mechanisms and Control (POF4-631) (POF4-631)
  2. 6G3 - PETRA III (DESY) (POF4-6G3) (POF4-6G3)
  3. FS-Proposal: I-20231381 (I-20231381) (I-20231381)
Experiment(s):
  1. PETRA Beamline P24 (PETRA III)

Appears in the scientific report 2025
Database coverage:
Medline ; Creative Commons Attribution CC BY 4.0 ; OpenAccess ; NationallizenzNationallizenz ; SCOPUS
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Synchrotron radiation instrumentation: proceedings, 15th international conference, SR>I 2024, Hamburg, Germany August 26-30, 2024
15th International Conference on Synchrotron Radiation Instrumentation, SRI 2024, HamburgHamburg, Germany, 26 Aug 2024 - 30 Aug 20242024-08-262024-08-30 Bristol, UK : IOP Publishing Ltd, Journal of Physics: Conference Series 3010 (2025), nonconsec. pag. ()  GO  Download fulltext Files  Download fulltextFulltext BibTeX | EndNote: XML, Text | RIS


 Record created 2025-06-10, last modified 2025-08-28


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