| Home > Publications database > A portable on-axis laser-heating system for near-90° X-ray spectroscopy: application to ferropericlase and iron silicide |
| Journal Article | PUBDB-2020-00771 |
; ; ; ; ; ; ; ; ; ; ; ; ; ; ; ; ; ; ; ;
2020
Wiley-Blackwell
[S.l.]
This record in other databases:
Please use a persistent id in citations: doi:10.1107/S1600577519017041 doi:10.3204/PUBDB-2020-00771
Abstract: A portable IR fiber laser-heating system, optimized for X-ray emission spectroscopy (XES) and nuclear inelastic scattering (NIS) spectroscopy with signal collection through the radial opening of diamond anvil cells near 90°with respect to the incident X-ray beam, is presented. The system offers double-sided on-axis heating by a single laser source and zero attenuation of incoming X-rays other than by the high-pressure environment. A description of the system, which has been tested for pressures above 100 GPa and temperatures up to 3000 K, is given. The XES spectra of laser-heated Mg0.67Fe0.33O demonstrate the potential to map the iron spin state in the pressure–temperature range of the Earth's lower mantle, and the NIS spectra of laser-heated FeSi give access to the sound velocity of this candidate of a phase inside the Earth's core. This portable system represents one of the few bridges across the gap between laser heating and high-resolution X-ray spectroscopies with signal collection near 90°.
|
The record appears in these collections: |