Journal Article

DESY-2014-03076

http://join2-wiki.gsi.de/foswiki/pub/Main/Artwork/join2_logo100x88.png Characterization of metal hydrides by in-situ XRD

Bösenberg, U.DESY* ; Pistidda, C.Extern* ; Tolkiehn, M.DESY* ; Busch, N.Extern* ; Saldan, I.Extern* ; Suarez-Alcantara, K.Extern* ; Arendarska, A.Extern* ; Klassen, T. ; Dornheim, M. (Corresponding Author)Extern*

2014
Elsevier New York, NY [u.a.]

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Please use a persistent id in citations: doi:10.1016/j.ijhydene.2014.02.068

Abstract: In-situ synchrotron radiation powder X-ray diffraction (SR-PXD) technique is a powerful tool to gain a deeper understanding of reaction mechanisms in crystalline materials. In this paper, the implementation of a new in-situ SR-PXD cell for solid–gas reactions is described in detail. The cell allows performing measurements in a range of pressure which goes from light vacuum (10−2 bar) up to 200 bar and temperatures from room temperature up to 550 °C. The high precision, with which pressure and temperature are measured, enables to estimate the thermodynamic properties of the observed changes in the crystal structure and phase transformations.

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Contributing Institute(s):

1. Experimentebetreuung PETRA III (FS-PE)
2. DOOR-User (DOOR)
3. FS-Experimentebetreuung DORIS (FS-DO)

Research Program(s):

1. DORIS Beamline D3 (POF2-54G13) (POF2-54G13)

Experiment(s):

1. DORIS Beamline D3 (DORIS III)

Appears in the scientific report 2014

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Database coverage:
; Current Contents - Social and Behavioral Sciences ; JCR ; NCBI Molecular Biology Database ; SCOPUS ; Science Citation Index ; Science Citation Index Expanded ; Thomson Reuters Master Journal List ; Web of Science Core Collection

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