TY  - JOUR
AU  - Bösenberg, Ulrike
AU  - Pistidda, Claudio
AU  - Tolkiehn, Martin
AU  - Busch, Nina
AU  - Saldan, Ivan
AU  - Suarez-Alcantara, Karina
AU  - Arendarska, Anna
AU  - Klassen, Thomas
AU  - Dornheim, Martin
TI  - Characterization of metal hydrides by in-situ XRD
JO  - International journal of hydrogen energy
VL  - 39
IS  - 18
SN  - 0360-3199
CY  - New York, NY [u.a.]
PB  - Elsevier
M1  - DESY-2014-03076
SP  - 9899 - 9903
PY  - 2014
AB  - In-situ synchrotron radiation powder X-ray diffraction (SR-PXD) technique is a powerful tool to gain a deeper understanding of reaction mechanisms in crystalline materials. In this paper, the implementation of a new in-situ SR-PXD cell for solid–gas reactions is described in detail. The cell allows performing measurements in a range of pressure which goes from light vacuum (10−2 bar) up to 200 bar and temperatures from room temperature up to 550 °C. The high precision, with which pressure and temperature are measured, enables to estimate the thermodynamic properties of the observed changes in the crystal structure and phase transformations.
LB  - PUB:(DE-HGF)16
UR  - <Go to ISI:>//WOS:000337859700041
DO  - DOI:10.1016/j.ijhydene.2014.02.068
UR  - https://bib-pubdb1.desy.de/record/170922
ER  -