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037 _ _ |a DESY-2014-03076
082 _ _ |a 660
100 1 _ |a Bösenberg, Ulrike
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245 _ _ |a Characterization of metal hydrides by in-situ XRD
260 _ _ |a New York, NY [u.a.]
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336 7 _ |a Journal Article
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520 _ _ |a In-situ synchrotron radiation powder X-ray diffraction (SR-PXD) technique is a powerful tool to gain a deeper understanding of reaction mechanisms in crystalline materials. In this paper, the implementation of a new in-situ SR-PXD cell for solid–gas reactions is described in detail. The cell allows performing measurements in a range of pressure which goes from light vacuum (10−2 bar) up to 200 bar and temperatures from room temperature up to 550 °C. The high precision, with which pressure and temperature are measured, enables to estimate the thermodynamic properties of the observed changes in the crystal structure and phase transformations.
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700 1 _ |a Pistidda, Claudio
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700 1 _ |a Tolkiehn, Martin
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700 1 _ |a Busch, Nina
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700 1 _ |a Saldan, Ivan
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700 1 _ |a Suarez-Alcantara, Karina
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700 1 _ |a Arendarska, Anna
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700 1 _ |a Klassen, Thomas
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700 1 _ |a Dornheim, Martin
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773 _ _ |a 10.1016/j.ijhydene.2014.02.068
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