Journal Article

DESY-2014-01462

http://join2-wiki.gsi.de/foswiki/pub/Main/Artwork/join2_logo100x88.png Aluminum-1,4-cyclohexanedicarboxylates: High-Throughput and Temperature-Dependent in Situ EDXRD Studies

Niekiel, F.Extern* ; Ackermann, M. ; Guerrier, P. ; Rothkirch, A.DESY* ; Stock, N. (Corresponding author)Extern*

2013
American Chemical Society Washington, DC

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Please use a persistent id in citations: doi:10.1021/ic400825b  doi:10.3204/DESY-2014-01462

Abstract: Exploring the use of the flexible aliphatic 1,4-cyclohexanedicarboxylic acid (H2CDC) as linker molecule in Al-MOF synthesis, two new compounds were discovered. The layered compound 1 is built from chains of corner-sharing AlO6-polyhedra and cis-CDC, while the microporous MIL-53 analogue CAU-13 (2) contains the same inorganic building unit as 1 but trans-CDC linker molecules in two different conformations. In addition to the detailed characterization of both compounds, the crystallization of 2 was investigated with temperature-dependent in situ EDXRD.

Note: © American Chemical Society

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Contributing Institute(s):

1. DOOR-User (DOOR)
2. FS-Experimentebetreuung DORIS (FS-DO)

Research Program(s):

1. DORIS Beamline F3 (POF2-54G13) (POF2-54G13)
2. PETRA Beamline P08 (POF2-54G14) (POF2-54G14)

Experiment(s):

1. DORIS Beamline F3 (DORIS III)
2. PETRA Beamline P08 (PETRA III)

Appears in the scientific report 2013

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Database coverage:
; ; JCR ; NCBI Molecular Biology Database ; Nationallizenz ; SCOPUS ; Science Citation Index ; Science Citation Index Expanded ; Thomson Reuters Master Journal List ; Web of Science Core Collection ; Zoological Record

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