Journal Article PUBDB-2025-02516

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Temperature-dependent deformation behavior of the additively manufactured Al$_{0.75}$CrFeNi$_{2.1}$ alloy using in-situ high energy X-ray diffraction

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2025
Elsevier Lausanne

Journal of alloys and compounds 1037, 182596 () [10.1016/j.jallcom.2025.182596]
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Abstract: Laser powder bed fusion of the hypo-eutectic eutectic alloy Al$_{0.75}$CrFeNi$_{2.1}$ conveniently produces an ultrafine quasi-lamellar microstructure composed of fcc and bcc phases. This is achieved by annealing the as-built and almost fully fcc microstructure, which has been published previously. In this study, two different annealing treatments were carried out, i.e. at 900 °C and 1000 °C for 6 h. The samples were compressed at temperatures up to 800 °C using in-situ high energy synchrotron X-ray diffraction (HEXRD). This technique provides studying macroscopic and phase-specific stress-strain evolution and therefore more insight into the stress partitioning as a function of test temperature between fcc A1 and bcc ordered B2. This analysis shows that below 400°C B2 is the major contributor to hardening, while above 600°C A1 contributes more, suggesting the softening of B2. The ultra-fine quasi-lamellar structure with confined B2 lamellae induces remarkably high dislocation density and hardening, as well as co-deformation of both phases. The dislocation density evolution was used to describe the macroscopic flow stress-strain using a phase fraction-weighted Taylor equation. The temperature capability of the novel material was compared with established materials and bridges the gap between steels and Ni-based alloys for applications up to 650 °C.

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Contributing Institute(s):
  1. DOOR-User (DOOR ; HAS-User)
  2. Helmholtz-Zentrum Hereon (Hereon)
Research Program(s):
  1. 6G3 - PETRA III (DESY) (POF4-6G3) (POF4-6G3)
  2. FS-Proposal: I-20221372 EC (I-20221372-EC) (I-20221372-EC)
Experiment(s):
  1. PETRA Beamline P07 (PETRA III)

Appears in the scientific report 2025
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Medline ; Clarivate Analytics Master Journal List ; Current Contents - Physical, Chemical and Earth Sciences ; Ebsco Academic Search ; Essential Science Indicators ; IF >= 5 ; JCR ; SCOPUS ; Science Citation Index Expanded ; Web of Science Core Collection
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 Record created 2025-07-28, last modified 2025-08-13


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