Journal Article PUBDB-2024-06442

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Correcting angular distortions in Bragg coherent X-ray diffraction imaging

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2024
Wiley-Blackwell [Erscheinungsort nicht ermittelbar]

Journal of synchrotron radiation 31(5), 1308-1316 () [10.1107/S1600577524006507]
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Abstract: Bragg coherent X-ray diffraction imaging (BCDI) has emerged as a powerful technique for strain imaging and morphology reconstruction of nanometre-scale crystals. However, BCDI often suffers from angular distortions that appear during data acquisition, caused by radiation pressure, heating or imperfect scanning stages. This limits the applicability of BCDI, in particular for small crystals and high-flux X-ray beams. Here, we present a pre-processing algorithm that recovers the 3D datasets from the BCDI dataset measured under the impact of large angular distortions. We systematically investigate the performance of this method for different levels of distortion and find that the algorithm recovers the correct angles for distortions up to 16.4× (1640%) the angular step size dθ = 0.004°. We also show that the angles in a continuous scan can be recovered with high accuracy. As expected, the correction provides marked improvements in the subsequent phase retrieval.

Classification:

Contributing Institute(s):
  1. DOOR-User (DOOR ; HAS-User)
  2. Experimentebetreuung PETRA III (FS-PET-S)
  3. FS-PETRA (FS-PETRA)
Research Program(s):
  1. 632 - Materials – Quantum, Complex and Functional Materials (POF4-632) (POF4-632)
  2. 6G3 - PETRA III (DESY) (POF4-6G3) (POF4-6G3)
  3. SWEDEN-DESY - SWEDEN-DESY Collaboration (2020_Join2-SWEDEN-DESY) (2020_Join2-SWEDEN-DESY)
  4. WIREDETECT - High resolution X-ray detectors based on nanowire arrays (801847) (801847)
  5. GenerationNano - Nanoscience doctoral training to address societal challenges in materials science, biomedicine and energy (945378) (945378)
Experiment(s):
  1. PETRA Beamline P10 (PETRA III)

Appears in the scientific report 2024
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 Record created 2024-10-24, last modified 2025-07-15


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