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@ARTICLE{Strapasson:639387,
author = {Strapasson, Guilherme and Arjona, Adrián S. and McPeak,
Joseph E. and Aalling-Frederiksen, Olivia and Sapnik, Adam
F. and Baun, Nanna L. and Bordallo, Heloisa N. and Rodella,
Cristiane B. and Zanchet, Daniela and Jensen, Kirsten M.
Ø.},
title = {{O}xygen {V}acancy-{I}nduced {P}hase {T}ransformations of
{I}ron-{D}oped {T}itanium {O}xide {N}anostructures},
journal = {ACS nano},
volume = {19},
number = {34},
issn = {1936-0851},
address = {Washington, DC},
publisher = {Soc.},
reportid = {PUBDB-2025-04481},
pages = {30986 - 30999},
year = {2025},
abstract = {Oxygen vacancies play a pivotal role in tailoring the
electronic, optical, and catalytic properties of reducible
metal oxides. Here, we provide a complete overview of oxygen
vacancy-induced structural evolution of iron-doped titanium
oxide nanomaterials with insights into their synthesis,
formation, and crystallization processes. Structural
analysis combining multiple techniques reveals the formation
of anatase nanoparticles at low Fe loadings (i.e., ≤10 at.
$\%$ Fe). At intermediate Fe concentrations (i.e., 15–20
at. $\%$ Fe), a mixture of anatase and rutile forms with the
presence of extended disordered defects similar to
crystallographic shear planes. These become more notable at
high Fe loadings (i.e., ≥30 at. $\%$ Fe) with the complete
transition to the rutile phase with a high density of
defects. Moreover, we provide important information on the
nucleation, growth, and crystallization processes during
synthesis, emphasizing the impact of Fe atom incorporation
on the TiO$_2$ lattice, the formation of reaction
intermediates, and the structural evolution at the nano
regime. The ability to control oxygen vacancies and engineer
defects in Fe-doped TiO$_2$ allows for the optimization of
charge transport, enhancing catalytic activity and tuning
optical properties for applications in environmental
remediation, sensing, and next-generation semiconductor
technologies.},
cin = {DOOR ; HAS-User},
ddc = {540},
cid = {I:(DE-H253)HAS-User-20120731},
pnm = {6G3 - PETRA III (DESY) (POF4-6G3) / FS-Proposal: I-20230285
EC (I-20230285-EC) / FS-Proposal: I-20230183 (I-20230183) /
MatMech - Live Tapings of Material Formation: Unravelling
formation mechanisms in materials chemistry through
Multimodal X-ray total scattering studies (804066)},
pid = {G:(DE-HGF)POF4-6G3 / G:(DE-H253)I-20230285-EC /
G:(DE-H253)I-20230183 / G:(EU-Grant)804066},
experiment = {EXP:(DE-H253)P-P02.1-20150101},
typ = {PUB:(DE-HGF)16},
doi = {10.1021/acsnano.5c08093},
url = {https://bib-pubdb1.desy.de/record/639387},
}