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@ARTICLE{Muoz:613801,
author = {Muñoz, Jairo Alberto and Barriobero-Vila, Pere and Stark,
Andreas and Schell, Norbert and Zhu, Yuntian and Cabrera,
José María},
title = {{S}oftening kinetics and mechanism during the annealing of
an {A}l-{S}i alloy produced by laser powder bed fusion},
journal = {Journal of alloys and compounds},
volume = {1005},
number = {176141},
issn = {0925-8388},
address = {Lausanne},
publisher = {Elsevier},
reportid = {PUBDB-2024-05628},
pages = {176141},
year = {2024},
note = {The Deutsches Elektronen-Synchrotron (DESY) is acknowledged
for theprovision of synchrotron radiation facilities in the
framework of the I-20221372 EC proposal. Waiting for
fulltext},
abstract = {This paper elucidates the softening kinetics during
isothermal annealing of an AlSi11 alloy manufactured by
laserpowder bed fusion (L-PBF) by using in situ high-energy
synchrotron X-ray diffraction complemented bymicrostructure
microscopy analysis. Annealing in the temperature range of
20 ◦C to 500 ◦C for one hour led toevolutions in the
as-built L-PBF cellular structure, including partial
fragmentation of the cell boundaries between20 ◦C and 300
◦C; the breakdown and transformation into ultrafine
Si-enriched particles in the range of 300 ◦C to400 ◦C;
and subsequently coarsening at temperatures exceeding 400
◦C. The evolution of the crystallite size for Siis
consistent with the Ostwald ripening equation with an
activation energy of 75.8 kJ mol 1, while the Al
peaksregistered only marginal variations through all the
thermal cycle. The examination of dislocation densities
andgrain sizes, which varied from 4 × 1014 m 2 to 1 ×
1014 m 2 and 15 μm to 13 μm respectively, in the
temperaturerange of 20 ◦C to 500 ◦C, revealed a
practical absence of recovery and recrystallization
phenomena in the Almatrix. On the other hand, Si diffusion
from the supersaturated Al matrix and the coalescence of
particles assistedthe cellular structure transformation.
Thus, the decrease in yield strength observed in the AlSi11
alloy subjectedto annealing treatments is primarily driven
by a thermally assisted softening process, which is
controlled by thediffusion of Si, rather than the
annihilation of dislocations and grain growth in the Al
matrix.},
cin = {DOOR ; HAS-User / Hereon},
ddc = {540},
cid = {I:(DE-H253)HAS-User-20120731 / I:(DE-H253)Hereon-20210428},
pnm = {6G3 - PETRA III (DESY) (POF4-6G3) / FS-Proposal: I-20221372
EC (I-20221372-EC)},
pid = {G:(DE-HGF)POF4-6G3 / G:(DE-H253)I-20221372-EC},
experiment = {EXP:(DE-H253)P-P07-20150101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:001312576900001},
doi = {10.1016/j.jallcom.2024.176141},
url = {https://bib-pubdb1.desy.de/record/613801},
}