Home > Publications database > Phase transition kinetics of superionic $H_2O$ ice phases revealed by MHz XFEL heating experiments > print

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024 7 _ |a 10.1038/s41467-024-52505-0
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100 1 _ |a Husband, Rachel
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245 _ _ |a Phase transition kinetics of superionic $H_2O$ ice phases revealed by MHz XFEL heating experiments
260 _ _ |a [London]
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500 _ _ |a We acknowledge support from the Deutsche For-schungsgemeinschaft (DFG) Research Unit FOR 2440 grants SA2585/5-1 (R.J.H, A.M., C.S.V., and H.P.L) and AP262/2-2 (K.A.).
520 _ _ |a H2O transforms to two forms of superionic (SI) ice at high pressures and temperatures, which contain highly mobile protons within a solid oxygen sublattice. Yet the stability field of both phases remains debated. Here, we present the results of an ultrafast X-ray heating study utilizing MHz pulse trains produced by the European X-ray Free Electron Laser to create high temperature states of H2O, which were probed using X-ray diffraction during dynamic cooling. We confirm an isostructural transition during heating in the 26-69 GPa range, consistent with the formation of SI-bcc. In contrast to prior work, SI-fcc was observed exclusively above ~50 GPa, despite evidence of melting at lower pressures. The absence of SI-fcc in these runs is attributed to short heating timescales and the pressure-temperature path induced by the pump-probe heating scheme in which H2O was heated above its melting temperature before the observation of quenched crystalline states, based on the earlier theoretical prediction that SI-bcc nucleates more readily from the fluid than SI-fcc. Our results may have implications for the stability of SI phases in ice-rich planets, for example during dynamic freezing, where the preferential crystallization of SI-bcc may result in distinct physical properties across mantle ice layers.
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536 _ _ |a DFG project 280637173 - FOR 2440: Materie im Inneren von Planeten - Hochdruck-, Planeten- und Plasmaphysik (280637173)
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542 _ _ |i 2024-09-23
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773 _ _ |a 10.1038/s41467-024-52505-0
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