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@ARTICLE{Pickhardt:597643,
      author       = {Pickhardt, Wilm and Siegfried, Eleonora and Fabig, Sven and
                      Rappen, Marisol Fabienne and Etter, Martin and Wohlgemuth,
                      Maximilian and Grätz, Sven and Borchardt, Lars},
      title        = {{T}he {S}onogashira {C}oupling on {P}alladium {M}illing
                      {B}alls—{A} new {R}eaction {P}athway in
                      {M}echanochemistry},
      journal      = {Angewandte Chemie},
      volume       = {62},
      number       = {27},
      issn         = {1433-7851},
      address      = {Weinheim},
      publisher    = {Wiley-VCH},
      reportid     = {PUBDB-2023-06638},
      pages        = {e202301490},
      year         = {2023},
      abstract     = {Utilizing direct mechanocatalytical conditions, the
                      Sonogashira coupling was successfully performed on the
                      surface of milling tools by using pure Pd and Pd coated
                      steel balls. The optimization of co-catalyst forming
                      additives led to a protocol, which generates quantitative
                      yields under aerobic conditions for various substrates
                      within as little as 90 minutes. Using state-of-the-art
                      spectroscopic, diffractive, as well as in situ methods lead
                      to the identification of a previously unknown and highly
                      reactive complex of the co-catalyst copper. This new complex
                      differs substantially from the known complexes in liquid
                      phase Sonogashira couplings, proving that reaction pathways
                      in mechanochemistry may differ from those in established
                      synthetic procedures.},
      cin          = {DOOR ; HAS-User / FS-PETRA-D},
      ddc          = {540},
      cid          = {I:(DE-H253)HAS-User-20120731 /
                      I:(DE-H253)FS-PETRA-D-20210408},
      pnm          = {631 - Matter – Dynamics, Mechanisms and Control
                      (POF4-631) / 6G3 - PETRA III (DESY) (POF4-6G3)},
      pid          = {G:(DE-HGF)POF4-631 / G:(DE-HGF)POF4-6G3},
      experiment   = {EXP:(DE-H253)P-P02.1-20150101},
      typ          = {PUB:(DE-HGF)16},
      pubmed       = {37018656},
      UT           = {WOS:000994540100001},
      doi          = {10.1002/anie.202301490},
      url          = {https://bib-pubdb1.desy.de/record/597643},
}