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@ARTICLE{Stolar:597157,
      author       = {Stolar, Tomislav and Alic, Jasna and Talajić, Gregor and
                      Cindro, Nikola and Rubčić, Mirta and Molčanov, Krešimir
                      and Uzarevic, Krunoslav and Hernandez, Jose},
      title        = {{S}upramolecular intermediates in thermo-mechanochemical
                      direct amidations},
      journal      = {Chemical communications},
      volume       = {59},
      number       = {90},
      issn         = {0022-4936},
      address      = {Cambridge},
      publisher    = {Soc.},
      reportid     = {PUBDB-2023-06447},
      pages        = {13490 - 13493},
      year         = {2023},
      note         = {Waiting for fulltext},
      abstract     = {We present a solvent-free thermo-mechanochemical approach
                      for the direct coupling of carboxylic acids and amines,
                      which avoids activators and additives. Detailed analysis of
                      the reactions by ex situ and in situ monitoring methods led
                      to the observation, isolation, and characterisation of
                      multicomponent crystalline intermediates that precede the
                      formation of amides. We applied our methodology for the
                      quantitative synthesis of the active pharmaceutical
                      ingredient moclobemide.},
      cin          = {DOOR ; HAS-User},
      ddc          = {540},
      cid          = {I:(DE-H253)HAS-User-20120731},
      pnm          = {6G3 - PETRA III (DESY) (POF4-6G3) / FS-Proposal: I-20220019
                      EC (I-20220019-EC)},
      pid          = {G:(DE-HGF)POF4-6G3 / G:(DE-H253)I-20220019-EC},
      experiment   = {EXP:(DE-H253)P-P02.1-20150101},
      typ          = {PUB:(DE-HGF)16},
      pubmed       = {37882212},
      UT           = {WOS:001087332000001},
      doi          = {10.1039/D3CC04448C},
      url          = {https://bib-pubdb1.desy.de/record/597157},
}