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000597157 1001_ $$0P:(DE-H253)PIP1083522$$aStolar, Tomislav$$b0$$eCorresponding author
000597157 245__ $$aSupramolecular intermediates in thermo-mechanochemical direct amidations
000597157 260__ $$aCambridge$$bSoc.$$c2023
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000597157 520__ $$aWe present a solvent-free thermo-mechanochemical approach for the direct coupling of carboxylic acids and amines, which avoids activators and additives. Detailed analysis of the reactions by ex situ and in situ monitoring methods led to the observation, isolation, and characterisation of multicomponent crystalline intermediates that precede the formation of amides. We applied our methodology for the quantitative synthesis of the active pharmaceutical ingredient moclobemide.
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000597157 7001_ $$0P:(DE-H253)PIP1100232$$aAlic, Jasna$$b1
000597157 7001_ $$00000-0002-7442-336X$$aTalajić, Gregor$$b2
000597157 7001_ $$00000-0001-9299-5815$$aCindro, Nikola$$b3
000597157 7001_ $$00000-0001-7239-4772$$aRubčić, Mirta$$b4
000597157 7001_ $$aMolčanov, Krešimir$$b5
000597157 7001_ $$0P:(DE-H253)PIP1026731$$aUzarevic, Krunoslav$$b6$$eCorresponding author
000597157 7001_ $$0P:(DE-H253)PIP1088073$$aHernandez, Jose$$b7$$eCorresponding author
000597157 773__ $$0PERI:(DE-600)1472881-3$$a10.1039/D3CC04448C$$gp. 10.1039.D3CC04448C$$n90$$p13490 - 13493$$tChemical communications$$v59$$x0022-4936$$y2023
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