Home > Publications database > In situ impregnated Ni/Al$_2$O$_3$ catalysts prepared by binder jet 3D printing using nickel nitrate-containing ink > print

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100 1 _ |a Bui, Hanh My
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245 _ _ |a In situ impregnated Ni/Al$_2$O$_3$ catalysts prepared by binder jet 3D printing using nickel nitrate-containing ink
260 _ _ |a Amsterdam
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520 _ _ |a The binder jetting printing technique enables in situ impregnation of alumina using a Ni(NOl$_3$)l$_2$-containing ink (NI), facilitating omission of impregnation. NI was compared to wet impregnation (WI). Full characterization by quasi-in situ XPS, XAS and TPR revealed the presence of Ni as NiAll$_2$Ol$_4$ spinel. TPR analysis identified surface NiO and NiAl$_2$Ol$_4$ species with facilitated reduction by NI, in addition to the respective species in bulk form. Post-processing affects active site accessibility by coverage. 3D printing limited the Ni loading, but XPS revealed higher metal dispersion by NI. COl$_2$ hydrogenation confirmed active Ni/All$_2$Ol$_3$ catalysts with enhanced activity by NI.
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700 1 _ |a Kratky, Tim
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700 1 _ |a Lee, Insu
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700 1 _ |a Khare, Rachit
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700 1 _ |a Hiller, Max
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700 1 _ |a Wedig, Steffen
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700 1 _ |a Günther, Sebastian
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700 1 _ |a Hinrichsen, Olaf
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773 _ _ |a 10.1016/j.catcom.2023.106738
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