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@ARTICLE{Shipilin:479518,
author = {Shipilin, Mikhail and Degerman, David and Lömker, Patrick
and Goodwin, Christopher M. and Rodrigues, Gabriel L. S. and
Wagstaffe, Michael and Gladh, Jörgen and Wang, Hsin-Yi and
Stierle, Andreas and Schlueter, Christoph and Pettersson,
Lars G. M. and Nilsson, Anders and Amann, Peter},
title = {{I}n {S}itu {S}urface-{S}ensitive {I}nvestigation of
{M}ultiple {C}arbon {P}hases on {F}e(110) in the
{F}ischer–{T}ropsch {S}ynthesis},
journal = {ACS catalysis},
volume = {12},
issn = {2155-5435},
address = {Washington, DC},
publisher = {ACS},
reportid = {PUBDB-2022-03141},
pages = {7609 - 7621},
year = {2022},
abstract = {Carbide formation on iron-based catalysts is an integral
and, arguably, the most important part of the
Fischer–Tropsch synthesis process, converting CO and H2
into synthetic fuels and numerous valuable chemicals. Here,
we report an in situ surface-sensitive study of the effect
of pressure, temperature, time, and gas feed composition on
the growth dynamics of two distinct iron–carbon phases
with the octahedral and trigonal prismatic coordination of
carbon sites on an Fe(110) single crystal acting as a model
catalyst. Using a combination of state-of-the-art X-ray
photoelectron spectroscopy at an unprecedentedly high
pressure, high-energy surface X-ray diffraction, mass
spectrometry, and theoretical calculations, we reveal the
details of iron surface carburization and product formation
under semirealistic conditions. We provide a detailed
insight into the state of the catalyst’s surface in
relation to the reaction.},
cin = {DOOR ; HAS-User / FS-PET-S / FS-NL},
ddc = {540},
cid = {I:(DE-H253)HAS-User-20120731 / I:(DE-H253)FS-PET-S-20190712
/ I:(DE-H253)FS-NL-20120731},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / 6G3 - PETRA III (DESY) (POF4-6G3) /
FS-Proposal: I-20200092 EC (I-20200092-EC) / FS-Proposal:
I-20181131 EC (I-20181131-EC) / SWEDEN-DESY - SWEDEN-DESY
Collaboration $(2020_Join2-SWEDEN-DESY)$ / CALIPSOplus -
Convenient Access to Light Sources Open to Innovation,
Science and to the World (730872)},
pid = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G3 /
G:(DE-H253)I-20200092-EC / G:(DE-H253)I-20181131-EC /
$G:(DE-HGF)2020_Join2-SWEDEN-DESY$ / G:(EU-Grant)730872},
experiment = {EXP:(DE-H253)P-P22-20150101 /
EXP:(DE-H253)P-P21.2-20150101},
typ = {PUB:(DE-HGF)16},
pubmed = {35815066},
UT = {WOS:000893251300001},
doi = {10.1021/acscatal.2c00905},
url = {https://bib-pubdb1.desy.de/record/479518},
}