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@ARTICLE{Nogly:309582,
author = {Nogly, Przemyslaw and Panneels, Valerie and Nelson, Garrett
and Gati, Cornelius and Kimura, Tetsunari and Milne,
Christopher and Milathianaki, Despina and Kubo, Minoru and
Wu, Wenting and Conrad, Chelsie and Coe, Jesse and Bean,
Richard and Zhao, Yun and Båth, Petra and Dods, Robert and
Harimoorthy, Rajiv and Beyerlein, Kenneth and Rheinberger,
Jan and James, Daniel and DePonte, Daniel and Li, Chufeng
and Sala, Leonardo and Williams, Garth J. and Hunter, Mark
S. and Koglin, Jason E. and Berntsen, Peter and Nango, Eriko
and Iwata, So and Chapman, Henry N. and Fromme, Petra and
Frank, Matthias and Abela, Rafael and Boutet, Sébastien and
Barty, Anton and White, Thomas and Weierstall, Uwe and
Spence, John and Neutze, Richard and Schertler, Gebhard and
Standfuss, Jörg},
title = {{L}ipidic cubic phase injector is a viable crystal delivery
system for time-resolved serial crystallography},
journal = {Nature Communications},
volume = {7},
issn = {2041-1723},
address = {London},
publisher = {Nature Publishing Group},
reportid = {PUBDB-2016-03927},
pages = {12314},
year = {2016},
abstract = {Serial femtosecond crystallography (SFX) using X-ray
free-electron laser sources is an emerging method with
considerable potential for time-resolved pump-probe
experiments. Here we present a lipidic cubic phase SFX
structure of the light-driven proton pump bacteriorhodopsin
(bR) to 2.3 Å resolution and a method to investigate
protein dynamics with modest sample requirement.
Time-resolved SFX (TR-SFX) with a pump-probe delay of 1 ms
yields difference Fourier maps compatible with the dark to M
state transition of bR. Importantly, the method is very
sample efficient and reduces sample consumption to about 1
mg per collected time point. Accumulation of M intermediate
within the crystal lattice is confirmed by time-resolved
visible absorption spectroscopy. This study provides an
important step towards characterizing the complete
photocycle dynamics of retinal proteins and demonstrates the
feasibility of a sample efficient viscous medium jet for
TR-SFX.},
cin = {FS-CFEL-1},
ddc = {500},
cid = {I:(DE-H253)FS-CFEL-1-20120731},
pnm = {6215 - Soft Matter, Health and Life Sciences (POF3-621) /
NANOMEM - Membrane Protein Nanocrystallography (317079) /
PSI-FELLOW - International Fellowship Program on Materials
$\&$ Matter, Energy $\&$ Environment, Human Health $\&$
Life-Sciences, and Accelerator Technology (290605) /
VH-GS-500 - PIER Helmholtz Graduate School
$(2015_IFV-VH-GS-500)$},
pid = {G:(DE-HGF)POF3-6215 / G:(EU-Grant)317079 /
G:(EU-Grant)290605 / $G:(DE-HGF)2015_IFV-VH-GS-500$},
experiment = {EXP:(DE-H253)CFEL-Exp-20150101 /
EXP:(DE-MLZ)External-20140101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000381904200001},
pubmed = {pmid:27545823},
doi = {10.1038/ncomms12314},
url = {https://bib-pubdb1.desy.de/record/309582},
}