Home > Publications database > In Situ Monitoring and Mechanism of the Mechanochemical Formation of a Microporous MOF-74 Framework > print |
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024 | 7 | _ | |a 10.1021/jacs.5b13038 |2 doi |
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100 | 1 | _ | |a Julien, Patrick A. |0 P:(DE-HGF)0 |b 0 |
245 | _ | _ | |a In Situ Monitoring and Mechanism of the Mechanochemical Formation of a Microporous MOF-74 Framework |
260 | _ | _ | |a Washington, DC |c 2016 |b American Chemical Society |
336 | 7 | _ | |a article |2 DRIVER |
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500 | _ | _ | |a (c) American Chemical Society. Post referee full text in progress (embargo 1 year from February 19, 2016). |
520 | _ | _ | |a Mechanochemistry provides a rapid, efficient route to metal−organic framework Zn-MOF-74 directly from a metal oxide and without bulk solvent.Insitu synchrotron X-ray diffraction monitoring of the reaction course reveals two new phases and an unusual stepwise process in which a close-packed intermediate reacts to form the open framework. The reaction can be performed on a gram scale to yield a highly porous material after activation. |
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700 | 1 | _ | |a Kimber, Simon A. J. |0 P:(DE-HGF)0 |b 3 |
700 | 1 | _ | |a Wang, Timothy |0 P:(DE-HGF)0 |b 4 |
700 | 1 | _ | |a Farha, Omar K. |0 P:(DE-HGF)0 |b 5 |
700 | 1 | _ | |a Zhang, Yuancheng |0 P:(DE-HGF)0 |b 6 |
700 | 1 | _ | |a Casaban, José |0 P:(DE-HGF)0 |b 7 |
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700 | 1 | _ | |a Etter, Martin |0 P:(DE-H253)PIP1018552 |b 9 |
700 | 1 | _ | |a Dinnebier, Robert |0 P:(DE-H253)PIP1018079 |b 10 |
700 | 1 | _ | |a James, Stuart L. |0 P:(DE-HGF)0 |b 11 |e Corresponding author |
700 | 1 | _ | |a Halasz, Ivan |0 P:(DE-HGF)0 |b 12 |e Corresponding author |
700 | 1 | _ | |a Friscic, Tomislav |0 P:(DE-H253)PIP1026729 |b 13 |e Corresponding author |
773 | _ | _ | |a 10.1021/jacs.5b13038 |g Vol. 138, no. 9, p. 2929 - 2932 |0 PERI:(DE-600)1472210-0 |n 9 |p 2929 - 2932 |t Journal of the American Chemical Society |v 138 |y 2016 |x 1520-5126 |
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