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@ARTICLE{Julien:308527,
author = {Julien, Patrick A. and Užarević, Krunoslav and Katsenis,
Athanassios D. and Kimber, Simon A. J. and Wang, Timothy and
Farha, Omar K. and Zhang, Yuancheng and Casaban, José and
Germann, Luzia S. and Etter, Martin and Dinnebier, Robert
and James, Stuart L. and Halasz, Ivan and Friscic, Tomislav},
title = {{I}n {S}itu {M}onitoring and {M}echanism of the
{M}echanochemical {F}ormation of a {M}icroporous {MOF}-74
{F}ramework},
journal = {Journal of the American Chemical Society},
volume = {138},
number = {9},
issn = {1520-5126},
address = {Washington, DC},
publisher = {American Chemical Society},
reportid = {PUBDB-2016-03738},
pages = {2929 - 2932},
year = {2016},
note = {(c) American Chemical Society. Post referee full text in
progress (embargo 1 year from February 19, 2016).},
abstract = {Mechanochemistry provides a rapid, efficient route to
metal−organic framework Zn-MOF-74 directly from a metal
oxide and without bulk solvent.Insitu synchrotron X-ray
diffraction monitoring of the reaction course reveals two
new phases and an unusual stepwise process in which a
close-packed intermediate reacts to form the open framework.
The reaction can be performed on a gram scale to yield a
highly porous material after activation.},
cin = {DOOR / FS-PE},
ddc = {540},
cid = {I:(DE-H253)HAS-User-20120731 / I:(DE-H253)FS-PE-20120731},
pnm = {6213 - Materials and Processes for Energy and Transport
Technologies (POF3-621) / 6G3 - PETRA III (POF3-622)},
pid = {G:(DE-HGF)POF3-6213 / G:(DE-HGF)POF3-6G3},
experiment = {EXP:(DE-H253)P-P02.1-20150101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000371945800015},
pubmed = {pmid:26894258},
doi = {10.1021/jacs.5b13038},
url = {https://bib-pubdb1.desy.de/record/308527},
}