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000308527 1001_ $$0P:(DE-HGF)0$$aJulien, Patrick A.$$b0
000308527 245__ $$aIn Situ Monitoring and Mechanism of the Mechanochemical Formation of a Microporous MOF-74 Framework
000308527 260__ $$aWashington, DC$$bAmerican Chemical Society$$c2016
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000308527 520__ $$aMechanochemistry provides a rapid, efficient route to metal−organic framework Zn-MOF-74 directly from a metal oxide and without bulk solvent.Insitu synchrotron X-ray diffraction monitoring of the reaction course reveals two new phases and an unusual stepwise process in which a close-packed intermediate reacts to form the open framework. The reaction can be performed on a gram scale to yield a highly porous material after activation.
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000308527 7001_ $$0P:(DE-H253)PIP1026731$$aUžarević, Krunoslav$$b1
000308527 7001_ $$0P:(DE-HGF)0$$aKatsenis, Athanassios D.$$b2
000308527 7001_ $$0P:(DE-HGF)0$$aKimber, Simon A. J.$$b3
000308527 7001_ $$0P:(DE-HGF)0$$aWang, Timothy$$b4
000308527 7001_ $$0P:(DE-HGF)0$$aFarha, Omar K.$$b5
000308527 7001_ $$0P:(DE-HGF)0$$aZhang, Yuancheng$$b6
000308527 7001_ $$0P:(DE-HGF)0$$aCasaban, José$$b7
000308527 7001_ $$0P:(DE-H253)PIP1026086$$aGermann, Luzia S.$$b8
000308527 7001_ $$0P:(DE-H253)PIP1018552$$aEtter, Martin$$b9
000308527 7001_ $$0P:(DE-H253)PIP1018079$$aDinnebier, Robert$$b10
000308527 7001_ $$0P:(DE-HGF)0$$aJames, Stuart L.$$b11$$eCorresponding author
000308527 7001_ $$0P:(DE-HGF)0$$aHalasz, Ivan$$b12$$eCorresponding author
000308527 7001_ $$0P:(DE-H253)PIP1026729$$aFriscic, Tomislav$$b13$$eCorresponding author
000308527 773__ $$0PERI:(DE-600)1472210-0$$a10.1021/jacs.5b13038$$gVol. 138, no. 9, p. 2929 - 2932$$n9$$p2929 - 2932$$tJournal of the American Chemical Society$$v138$$x1520-5126$$y2016
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