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@ARTICLE{Beyerlein:291710,
      author       = {Beyerlein, Kenneth and Adriano, L. and Heymann, M. and
                      Kirian, R. and Knoška, J. and Wilde, F. and Chapman, H. N.
                      and Bajt, Sasa},
      title        = {{C}eramic micro-injection molded nozzles for serial
                      femtosecond crystallography sample delivery},
      journal      = {Review of scientific instruments},
      volume       = {86},
      number       = {12},
      issn         = {1089-7623},
      address      = {[S.l.]},
      publisher    = {American Institute of Physics},
      reportid     = {PUBDB-2015-05540},
      pages        = {125104 -},
      year         = {2015},
      abstract     = {Serial femtosecond crystallography (SFX) using X-ray
                      Free-Electron Lasers (XFELs) allows for room temperature
                      protein structure determination without evidence of
                      conventional radiation damage. In this method, a liquid
                      suspension of protein microcrystals can be delivered to the
                      X-ray beamin vacuum as a micro-jet, which replenishes the
                      crystals at a rate that exceeds the current XFEL pulse
                      repetition rate. Gas dynamic virtual nozzles produce the
                      required micrometer-sized streams by the focusing action of
                      a coaxial sheath gas and have been shown to be effective for
                      SFXexperiments. Here, we describe the design and
                      characterization of such nozzles assembled from ceramic
                      micro-injection molded outer gas-focusing capillaries.
                      Trends of the emitted jet diameter and jet length as a
                      function of supplied liquid and gas flow rates are measured
                      by a fast imagingsystem. The observed trends are explained
                      by derived relationships considering choked gas flow and
                      liquid flow conservation. Finally, the performance of these
                      nozzles in a SFX experiment is presented, including an
                      analysis of the observed background.},
      cin          = {FS-CFEL-1 / FS-ML},
      ddc          = {530},
      cid          = {I:(DE-H253)FS-CFEL-1-20120731 / I:(DE-H253)FS-ML-20120731},
      pnm          = {6215 - Soft Matter, Health and Life Sciences (POF3-621) /
                      6G3 - PETRA III (POF3-622) / 05E13GU1 - Entwicklung eines
                      "Serial Femtosecond Crystallography (SFX)"-Messtandes am
                      Europäischen Elektronenlaser XFEL (BMBF-05E13GU1)},
      pid          = {G:(DE-HGF)POF3-6215 / G:(DE-HGF)POF3-6G3 /
                      G:(DE-H253)BMBF-05E13GU1},
      experiment   = {EXP:(DE-H253)P-P05-20150101 /
                      EXP:(DE-H253)CFEL-Exp-20150101},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000368594900072},
      pubmed       = {pmid:26724070},
      doi          = {10.1063/1.4936843},
      url          = {https://bib-pubdb1.desy.de/record/291710},
}