TY - JOUR
AU - Nogly, Przemyslaw
AU - James, Daniel
AU - Wang, Dingjie
AU - White, Thomas A.
AU - Zatsepin, Nadia
AU - Shilova, Anastasya
AU - Nelson, Garrett
AU - Liu, Haiguang
AU - Johansson, Linda
AU - Heymann, Michael
AU - Jaeger, Kathrin
AU - Metz, Markus
AU - Wickstrand, Cecilia
AU - Wu, Wenting
AU - Båth, Petra
AU - Berntsen, Peter
AU - Oberthuer, Dominik
AU - Panneels, Valerie
AU - Cherezov, Vadim
AU - Chapman, Henry
AU - Schertler, Gebhard
AU - Neutze, Richard
AU - Spence, John
AU - Moraes, Isabel
AU - Burghammer, Manfred
AU - Standfuss, Joerg
AU - Weierstall, Uwe
TI - Lipidic Cubic Phase Serial Millisecond Crystallography using Synchrotron Radiation
JO - IUCrJ
VL - 2
IS - 2
SN - 2052-2525
CY - Chester
PB - International Union of Crystallography (IUCr)
M1 - PUBDB-2015-01346
SP - 168 - 176
PY - 2015
N1 - PIF-2015-46
AB - Lipidic cubic phases (LCPs) have emerged as successful matrixes for the crystallization of membrane proteins.Moreover, the viscous LCP also provides a highly effective delivery medium for serial femtosecond crystallography (SFX) at X-ray free-electron lasers (XFELs). Here, the adaptation of this technology to perform serial millisecond crystallography (SMX) at more widely available synchrotron microfocus beamlines is described. Compared with conventional microcrystallography, LCP-SMX eliminates the need for difficult handling of individual crystals and allows for data collection at room temperature. The technology is demonstrated by solving a structure of the light-driven protonpump bacteriorhodopsin (bR) at a resolution of 2.4 A ° . The room-temperature structure of bR is very similar to previous cryogenic structures but shows small yet distinct differences in the retinal ligand and proton-transfer pathway.
LB - PUB:(DE-HGF)16
UR - <Go to ISI:>//WOS:000356866400007
C6 - pmid:25866654
DO - DOI:10.1107/S2052252514026487
UR - https://bib-pubdb1.desy.de/record/207438
ER -