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@ARTICLE{Scherdel:87608,
      author       = {Scherdel, C. and Scherb, T. and Reichenauer, G. and DESY},
      title        = {{S}pherical porous carbon particles derived from
                      suspensions and sediments of resorcinol-formaldehyde
                      particles},
      journal      = {Carbon},
      volume       = {47},
      issn         = {0008-6223},
      address      = {Amsterdam [u.a.]},
      publisher    = {Elsevier Science},
      reportid     = {PHPPUBDB-9962},
      pages        = {2244-2252},
      year         = {2009},
      note         = {© Elsevier Ltd. ; Post referee fulltext in progress 2;
                      Embargo 12 months from publication},
      abstract     = {The goal of this study is the completion of the parameter
                      field of resorcinol–formaldehyde solutions towards the
                      regime of non-monolithic phases. For low sodium carbonate
                      concentration and low mass content of resorcinol and
                      formaldehyde in the starting solution the formation of
                      spherical particles rather than monolithic gels is observed.
                      The organic precursors were converted into carbon powders by
                      pyrolysis. The resulting carbon particles were characterized
                      by scanning electron microscopy (SEM), nitrogen sorption and
                      small-angle X-ray scattering (SAXS). The study shows that
                      carbonization of the organic particles results in spherical
                      carbon particles with a micropore volume of about 0.28
                      cm3/g. The composition of the starting solution, however,
                      strongly affects the external surface area as determined
                      from sorption data for the organic as well as for the
                      corresponding carbon particles; the values derived can be
                      converted into average diameters of spherical particles
                      ranging from 30 nm to 5 μm. Complementary SEM and SAXS
                      measurements confirm these findings. A diameter of 5 μm
                      appears to be the upper size limit in particle size forming,
                      while 30 nm spheres develop near the formation of a
                      continuous gel at relatively high sodium carbonate
                      concentrations.},
      cin          = {HASYLAB(-2012)},
      ddc          = {540},
      cid          = {$I:(DE-H253)HASYLAB_-2012_-20130307$},
      pnm          = {DORIS Beamline BW4 (POF1-550) / DORIS Beamline B1
                      (POF1-550) / FS-Proposal: II-20052060 (II-20052060)},
      pid          = {G:(DE-H253)POF1-BW4-20130405 / G:(DE-H253)POF1-B1-20130405
                      / G:(DE-H253)II-20052060},
      experiment   = {EXP:(DE-H253)D-BW4-20150101 / EXP:(DE-H253)D-B1-20150101},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000267965200020},
      doi          = {10.1016/j.carbon.2009.04.015},
      url          = {https://bib-pubdb1.desy.de/record/87608},
}