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@INPROCEEDINGS{Zaluzhnyy:644511,
author = {Zaluzhnyy, Ivan and Schreiber, Frank and Rysov, Rustam and
Unger, Frederik and Kneschaurek, Ekaterina and Hagara, Jakub
and Zimmermann, Paul and Schwartzkopff, Sebastian and
Pithan, Linus and Lapkin, Dmitry and Hinderhofer, Alexander
and Westermeier, Fabian and Sprung, Michael and Vaynzof,
Yana and Paulus, Fabian and Merten, Lena},
title = {{D}ynamics and kinetics of light-induced phase segregation
in mixed lead-halide perovskites},
reportid = {PUBDB-2026-00370},
year = {2025},
note = {kein PDF download angeboten, nur online lesbar},
abstract = {Hybrid organic-inorganic perovskites tend to undergo
several structural transformations that can be caused by
temperature, humidity and light. One of the striking is
light-induced halide phase segregation in mixed lead-halide
perovskites, i.e., formation of I-rich and Br-rich domains
by the illumination with visible light [1]. This effect
influences the homogeneity of the chemical composition of
the mixed perovskite phase, influence the band gaps and
therefore it has strong impact on the perovskite-based
photovoltaic devices. Several microscopic mechanisms have
been proposed to explain this effect, but the full
understanding is yet to be obtained [2].In this work, we
used X-ray photon correlation spectroscopy (XPCS) [3], to
perform time-resolved studies of the light-induced phase
segregation in (CH3NH3)PbBr1.8I1.2 [4] and track the
formation of pure (CH3NH3)PbBrI3 and (CH3NH3)PbI3. This was
done by observing the (001) diffraction peak from the cubic
perovskite lattice and, specifically, quantifying the
dynamics of coherent speckles originating from domains with
different halide concentration.We observe that the phase
segregation is characterized by three distinct time scales
corresponding to the rapid formation of small seeds of the
I-rich phase, fluctuations of the ion distribution around
the quasi-equilibrium state (dynamics), and a directional
drift of the ions within the crystal grains (kinetics). We
also investigate a series of samples with interstitials and
vacancies in the halide sublattice [5] and observe the
influence of defects in the halide sublattice on phase
separation. We find that samples with interstitial halides
exhibit slower phase separation as samples with vacancies in
the halide sublattice.},
month = {Sep},
date = {2025-09-08},
organization = {Perovskite Semiconductors: From
Fundamental Properties to Devices,
Konstanz (Germany), 8 Sep 2025 - 10 Sep
2025},
cin = {DOOR ; HAS-User / FS-EC / FS-PET-S},
cid = {I:(DE-H253)HAS-User-20120731 / I:(DE-H253)FS-EC-20120731 /
I:(DE-H253)FS-PET-S-20190712},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / 6G3 - PETRA III (DESY) (POF4-6G3)},
pid = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G3},
experiment = {EXP:(DE-H253)P-P10-20150101},
typ = {PUB:(DE-HGF)6},
doi = {10.29363/nanoge.perfunpro.2025.038},
url = {https://bib-pubdb1.desy.de/record/644511},
}