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@ARTICLE{Seitz:640123,
author = {Seitz, Philipp and Rzesny, Luisa and Busse, Darleen and
Xiang, Xiaoshuang and Hermann, Mathias and Estaque, Lilian
and Pieters, Grégory and Esser, Birgit},
title = {{S}ize and {G}eometry {I}mpact the {C}hiroptical
{P}roperties of {D}ouble {N}anohoops},
journal = {Journal of the American Chemical Society},
volume = {147},
number = {45},
issn = {0002-7863},
address = {Washington, DC},
publisher = {ACS Publications},
reportid = {PUBDB-2025-04709},
pages = {41610 - 41619},
year = {2025},
abstract = {: Conjugated nanohoops have attracted much attention in
recent years due to their unique optoelectronic
properties.Amorecomplexgeometry, inwhichtwonanohoopsare
covalentlylinkedtoformaso-calleddoublenanohoop,canhavea
significant influenceon themorphology, (chir)optical
properties andsupramolecular interactions comparedtoa
singlenanohoop. Herein,wepresent thesystematicdesign,
synthesis, structuraland chiroptical analysis of a novel
series of three chiral double nanohoops togetherwiththeir
singlehoopreferencecompounds. Theyeach incorporatea
tetrahydroindeno[2,1-a]indene-5,10-diol unit
asanasymmetricbridgewithcentral chirality.Notably, they
$displayhighphotoluminescencequantumyieldsof79−95\%,alongwithdistincttrendsinabsorption,emission,andenergytransfer$
dynamics.EnantiomersofthedoubleandreferencesinglenanohoopsweresuccessfullyseparatedbyHPLCusingachiralstationary
phase, and their chiroptical propertieswere investigated
throughelectronic circular dichroism(ECD)
andcircularlypolarized
luminescence(CPL)spectroscopyrevealingincreasedasymmetryfactors(gabs)comparedtotheirreferencecompounds.Ourstudy
provides a systematic explorationof howsize, geometry,
andasymmetry impact theoptoelectronic behavior of chiral
double nanohoopsandoffersvaluable insight for
thedevelopmentofhigh-performancechiropticalmaterials.},
cin = {DOOR ; HAS-User},
ddc = {540},
cid = {I:(DE-H253)HAS-User-20120731},
pnm = {6G3 - PETRA III (DESY) (POF4-6G3) / FS-Proposal: R-20241280
(R-20241280) / DFG project G:(GEPRIS)434040413 -
Pentalenbasierte antiaromatische Nanoreifen und Nanogürtel
(PANEL) (434040413) / DFG project G:(GEPRIS)446026621 -
ORGanische ANIONen-“Rocking-Chair”-Batterien mit kleinen
Molekülen als Elektrodenmaterialien und ihre
Leistungsevaluation (446026621) / DFG project
G:(GEPRIS)528773185 - MALDI-TOF/TOF Massenspektrometer
(528773185) / DFG project 445470598 - 600 MHz-NMR-Gerät mit
Stickstoff-gekühltem Probenkopf (445470598) / DFG project
445471097 - 400 MHz-NMR-Konsole mit
Festkörper-Probenköpfen (445471097) / DFG project
445471845 - 400 MHz-NMR-Konsole mit Breitband-Probenkopf
(445471845) / DFG project G:(GEPRIS)534044797 - Large Scale
Data Facility 3 - Anteil Forschungsgroßgerät (LSDF3-FuGG)
(534044797)},
pid = {G:(DE-HGF)POF4-6G3 / G:(DE-H253)R-20241280 /
G:(GEPRIS)434040413 / G:(GEPRIS)446026621 /
G:(GEPRIS)528773185 / G:(GEPRIS)445470598 /
G:(GEPRIS)445471097 / G:(GEPRIS)445471845 /
G:(GEPRIS)534044797},
experiment = {EXP:(DE-H253)P-P24-20150101},
typ = {PUB:(DE-HGF)16},
doi = {10.1021/jacs.5c12590},
url = {https://bib-pubdb1.desy.de/record/640123},
}