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@ARTICLE{Lee:639756,
      author       = {Lee, Yun-Hee and Kim, Jin Kyun and Kim, Yongkyu and Kim,
                      Minju and CHO, DEOK-YONG and Husband, Rachel J. and Strohm,
                      Cornelius and Ehrenreich-Petersen, Emma and Glazyrin,
                      Konstantin and Laurus, Torsten and Graafsma, Heinz and
                      Bauer, Robert and Lehmkühler, Felix and Appel, Karen and
                      Konôpková, Zuzana and Tang, Minxue and Dwivedi, Anand and
                      Sztuck-Dambietz, Jolanta and Randolph, Lisa and Buakor,
                      Khachiwan and Humphries, Oliver and Baehtz, Carsten and
                      Eklund, Tobias and Mohrbach, Lisa Katharina and Mondal,
                      Anshuman and Marquardt, Hauke and O’Bannon, Earl Francis
                      and Amann-Winkel, Katrin and Yoo, Choong-Shik and Zastrau,
                      Ulf and Liermann, Hanns-Peter and Nada, Hiroki and Lee, Geun
                      Woo},
      title        = {{M}ultiple freezing–melting pathways of high-density ice
                      through ice {XXI} phase at room temperature},
      journal      = {Nature materials},
      volume       = {xxx},
      number       = {xxx},
      issn         = {1476-1122},
      address      = {Basingstoke},
      publisher    = {Nature Publishing Group},
      reportid     = {PUBDB-2025-04651},
      pages        = {xxx},
      year         = {2025},
      note         = {OnlineFirst VDB},
      abstract     = {Various metastable ice phases and their complicated
                      transition pathwayshave been found by pressurization at low
                      temperatures at which slowkinetics and high metastability
                      are easily achieved. By contrast, suchdiversity is less
                      expected at room or elevated temperatures. Here, using
                      acombination of a dynamic diamond anvil cell and X-ray free
                      electron lasertechniques, we demonstrate t ha t sup erco mp
                      ressed water transforms intoice VI through multiple
                      freezing–melting pathways at room temperature,hidden
                      within the pressure region of ice VI. These multiple
                      transitionpathways occur via a metastable ice (more
                      specifically, ice XXI withbody-centred tetragonal structure
                      (Ī 42d)) discovered in this study and ametastable ice VII
                      that exists within the pressure range of ice VI. We find
                      thatsupercompressed water structurally evolves from
                      high-density water tovery-high-density water, causing
                      multiple transition pathways. Thesefindings provide an
                      insight to find more metastable ice phases and
                      theirtransition pathways at elevated temperatures.},
      cin          = {FS-PETRA-D / FS-HIBEF / DOOR ; HAS-User / FS-DS /
                      $XFEL_DO_DD_DET$ / FS-SMP / $XFEL_E1_FXE$ / $XFEL_E1_HED$},
      ddc          = {610},
      cid          = {I:(DE-H253)FS-PETRA-D-20210408 /
                      I:(DE-H253)FS-HIBEF-20240110 / I:(DE-H253)HAS-User-20120731
                      / I:(DE-H253)FS-DS-20120731 /
                      $I:(DE-H253)XFEL_DO_DD_DET-20210408$ /
                      I:(DE-H253)FS-SMP-20171124 /
                      $I:(DE-H253)XFEL_E1_FXE-20210408$ /
                      $I:(DE-H253)XFEL_E1_HED-20210408$},
      pnm          = {631 - Matter – Dynamics, Mechanisms and Control
                      (POF4-631) / 6G3 - PETRA III (DESY) (POF4-6G3) /
                      FS-Proposal: I-20240991 (I-20240991) / DFG project
                      G:(GEPRIS)329658874 - Experimentelle Untersuchung von
                      planetaren Eis-Verbindungen bei hohen Drücken mittels
                      dynamisch-betriebener Diamantstempelzellen (329658874) /
                      HiBEF - HIBEF Consortium $(2020_Join2-HiBEF)$ / DFG project
                      G:(GEPRIS)390715994 - EXC 2056: CUI: Tiefe Einblicke in
                      Materie (390715994) / FS-Proposal: I-20220299 (I-20220299) /
                      FS-Proposal: I-20221305 (I-20221305)},
      pid          = {G:(DE-HGF)POF4-631 / G:(DE-HGF)POF4-6G3 /
                      G:(DE-H253)I-20240991 / G:(GEPRIS)329658874 /
                      $G:(DE-HGF)2020_Join2-HiBEF$ / G:(GEPRIS)390715994 /
                      G:(DE-H253)I-20220299 / G:(DE-H253)I-20221305},
      experiment   = {EXP:(DE-H253)P-P02.2-20150101 /
                      EXP:(DE-H253)XFEL-HED-20150101},
      typ          = {PUB:(DE-HGF)16},
      doi          = {10.1038/s41563-025-02364-x},
      url          = {https://bib-pubdb1.desy.de/record/639756},
}