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@ARTICLE{Stber:639645,
author = {Stüber, Alexander and Jurgeleit, Ramona and Berger, Kira
and Grimm-Lebsanft, Benjamin and Buchenau, Sören and Senft,
Laura and Näther, Christian and Ivanović-Burmazović,
Ivana and Rübhausen, Michael and Naumova, Maria and Tuczek,
Felix},
title = {{V}ariable {C}oordination of {P}eroxide in a {D}inuclear
{C}opper {M}ono‐{O}xygenase {M}odel {C}omplex {S}upported
by a {P}yridazine‐{B}ridged {L}igand},
journal = {European journal of inorganic chemistry},
volume = {28},
number = {28},
issn = {1434-1948},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {PUBDB-2025-04602},
pages = {e202500286},
year = {2025},
note = {cc-by},
abstract = {Copper-oxygen intermediates play an important role in
nature as active species of many copper-containing enzymes.
However, copper-oxygen intermediates have a key function not
only in nature, but also in industry, for example as
catalysts. Herein a study on a dinuclear copper complex is
presented based on the literature known ligand BPMPD. This
ligand combines features of the previously investigated
systems (octadentate N-donor, like the MO8 system and
pyridine donors, like the bdpdz system). Oxygenation of the
Cu(I)-complex with O$_2$ at low temperature leads to the
formation of a μ-1,2-peroxo intermediate (Cu$_2$O$_2$),
which is characterized with UV/Vis-, rRaman- and X-ray
absorption spectroscopy (XAS), as well as by
cryo-UHR-electrospray ionization mass spectrometry. The
Cu$_2$O$_2$ species can be reversibly converted into a
μ-1,1-hydroperoxo intermediate (Cu$_2$OOH) by a reaction
with lutidinium triflate and
1,8-diazabicyclo[5.4.0]undec-7-ene (DBU), which can be
monitored by UV/Vis and XAS. Furthermore, the reactivity of
the Cu$_2$O$_2$ species toward dihydroanthracene is
investigated.},
cin = {DOOR ; HAS-User / FS-PETRA-S},
ddc = {540},
cid = {I:(DE-H253)HAS-User-20120731 /
I:(DE-H253)FS-PETRA-S-20210408},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / 6G3 - PETRA III (DESY) (POF4-6G3) /
DFG project G:(GEPRIS)458902672 - Exom-Sequenzierung für
Patienten mit chronisch entzündlichen Darmerkrankungen, die
mit Biologika behandelt wurden (458902672)},
pid = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G3 /
G:(GEPRIS)458902672},
experiment = {EXP:(DE-H253)P-P65-20150101},
typ = {PUB:(DE-HGF)16},
doi = {10.1002/ejic.202500286},
url = {https://bib-pubdb1.desy.de/record/639645},
}