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@ARTICLE{Ercan:639428,
author = {Ercan, Kerem Emre and Karatok, Mustafa and Say, Zafer and
Kurt, Merve and Sika-Nartey, Abel Tetteh and Ozensoy, Emrah},
title = {{C}ooperative {C}atalytic {R}ole of {C}o and {M}n {S}ites
on {L}a{C}o$_x${M}n$_{1–x}${O}$_3$ {P}erovskite
{N}anoparticles in {CO} and {NO} {O}xidation},
journal = {ACS applied nano materials},
volume = {8},
number = {34},
issn = {2574-0970},
address = {Washington, DC},
publisher = {ACS Publications},
reportid = {PUBDB-2025-04520},
pages = {16779 - 16791},
year = {2025},
abstract = {Perovskites have significant potential to improve
efficiency, reduce the costs of conventional oxidation
catalysts, and contribute to cleaner and more sustainable
energy solutions. However, numerous structural factors
influencing their catalytic performance are still a subject
to debate. In this study, simple perovskite nanoparticles in
the form of LaCoO3 (LC) and LaMnO3 (LM), as well as
LaCoxMn1–xO3 (LCM)-mixed B-site perovskites with different
B-site cations, were synthesized and their performances in
CO oxidation and NO oxidation reactions were examined. The
LaCo0.8Mn0.2O3 catalyst exhibited the highest catalytic
activity in both CO and NO oxidation reactions, surpassing
the 1 wt $\%Pt/γ-Al2O3$ benchmark nanoparticle catalyst and
other currently investigated perovskite nanoparticles. Co
sites (predominantly Co3+) in the optimized LaCo0.8Mn0.2O3
catalyst were found to be enriched in electron density,
while Mn sites (mostly in Mn4+ form) were found to be more
electron deficient as opposed to LC and LM. LaCo0.8Mn0.2O3
not only released significantly greater amounts of oxygen
and generated larger extents of oxygen vacancies than LC and
LM under reducing conditions but also achieved this at
favorably lower temperatures. In light of the current
results, we report that Co sites in LCM operate as the main
active site during both CO and NO oxidation by enabling
stabilization and activation of O2 (ads), while Mn sites
mainly serve as promoters by increasing the adsorption
strength of CO (ads) and NO (ads) as well as facilitating
oxygen vacancy formation and vacancy regeneration, where
oxygen vacancies were also found to contribute particularly
to the NO oxidation reaction within the currently
investigated thermal window. These findings demonstrate that
the electronic properties of LCM can be systematically
tailored at the nanometer scale in a versatile manner to
address different reactivity requirements of challenging
catalytic reactions.},
cin = {DOOR ; HAS-User},
ddc = {540},
cid = {I:(DE-H253)HAS-User-20120731},
pnm = {6G3 - PETRA III (DESY) (POF4-6G3) / CALIPSOplus -
Convenient Access to Light Sources Open to Innovation,
Science and to the World (730872)},
pid = {G:(DE-HGF)POF4-6G3 / G:(EU-Grant)730872},
experiment = {EXP:(DE-H253)P-P65-20150101},
typ = {PUB:(DE-HGF)16},
doi = {10.1021/acsanm.5c02876},
url = {https://bib-pubdb1.desy.de/record/639428},
}