% IMPORTANT: The following is UTF-8 encoded. This means that in the presence % of non-ASCII characters, it will not work with BibTeX 0.99 or older. % Instead, you should use an up-to-date BibTeX implementation like “bibtex8” or % “biber”. @PHDTHESIS{Mueller:639107, author = {Mueller, Simon}, othercontributors = {Reinert, Friedrich and Brunner, Karl}, title = {{I}ntermediate valence transition in epitaxial (111) films of strongly correlated {T}hulium monochalcogenides{Z}wischenvalenz-Übergänge in epitaktischen (111) {F}ilmen aus stark korrelierten {T}hulium-{M}onochalkogeniden}, school = {Julius-Maximilians-Universitaet Wuerzburg}, type = {Dissertation}, address = {Wuerzburg}, publisher = {Universität Würzburg}, reportid = {PUBDB-2025-04310}, pages = {158}, year = {2025}, note = {Dissertation, Julius-Maximilians-Universitaet Wuerzburg, 2024}, abstract = {Fundamental insights into complex quantum phases of many-body systems can be ob-tained by the investigation of the underlying particle interactions. The variety of compet-ing interactions between particles involved determines their behaviour in these quantumphases. In strongly correlated electron systems the involved particles are the localized4f-electrons and the itinerant 5d-electrons. Their interactions can lead to the fascinatingintermediate valence phase of non-integer f-occupation. In TmSe1−xTex this phase canbe induced by a semiconductor-metal transition whose volume change already indicates adrastic change in electron interaction. This phase transition makes TmSe1−xTex suitableto investigate the evolution of the electron interactions. The major issue is the unavail-ability of TmSe1−xTex crystals within the phase transition due to a miscibility gap justlocated around the point of transition. In order to close this gap and realize TmSe1−xTexcompounds throughout the whole semiconductor-metal transition, the epitaxial growthof TmSe1−xTex by molecular-beam epitaxy is chosen. The advantage of this system isthe unique possibility to study the evolution of the electron interactions by photoemissionspectroscopy since the whole phase transition and thus the emergence of intermediatevalence appears under ambient conditions. Systematic investigations on this phase tran-sition in epitaxial TmSe1−xTex have not yet been realised by photoemission spectroscopywhich is therefore the task of this work. For this purpose, a high quality epitaxial growthof TmSe1−xTex is achieved on SrF2 (111) which in addition opens a spectroscopic accessso far unavailable by bulk single crystal cleavage. Two strategies to obtain TmSe1−xTexphases throughout the phase transition are investigated. Tuning the lattice parameters ofTmTe by substrate-induced strain turns out to be not enough to reach the phase transi-tion. A direct growth of thin TmSe1−xTex films varying in xenables the investigation of theoverall electronic structure across the phase transition although the miscibility gap is notclosed by epitaxy. This includes the first ever observed bandstructure of TmTe and TmSein the (111) orientation. In the metallic phase of the transition a constant f-occupation isobserved while in the semiconducting phase the f-occupation seems to decrease towardsthe phase transition. Drastic variations in the electronic interactions are hereby displayedwhich are accompanied by the observed gap opening. The detected separation of the 4f-state in the intermediate valence phase at temperatures below 100 K is unexpected by theunderlying Anderson model. It shows the possibly necessary inclusion of other interac-tions among the electrons for the theoretical description of intermediate valence systems.With these results the basis for further investigations of electron interactions in the inter-mediate valence system TmSe1−xTex is given. The goal to provide spectroscopic access bymolecular-beam epitaxy to phases throughout the transition has not been ruled out.}, cin = {FS-SXQM}, ddc = {530 Physik}, cid = {I:(DE-H253)FS-SXQM-20190201}, pnm = {632 - Materials – Quantum, Complex and Functional Materials (POF4-632) / 6G3 - PETRA III (DESY) (POF4-6G3) / FS-Proposal: I-20231357 (I-20231357) / FS-Proposal: I-20200225 (I-20200225)}, pid = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G3 / G:(DE-H253)I-20231357 / G:(DE-H253)I-20200225}, experiment = {EXP:(DE-H253)P-P04-20150101 / EXP:(DE-H253)P-P08-20150101}, typ = {PUB:(DE-HGF)11}, urn = {urn:nbn:de:bvb:20-opus-404035}, url = {https://bib-pubdb1.desy.de/record/639107}, }