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@ARTICLE{Gubicza:638438,
author = {Gubicza, Jeno and Mathis, Kristian and Nagy, Peter and
Jenei, Péter and Hegedues, Zoltan and Farkas, Andrea and
Veselý, Jozef and Inoue, Shin-ichi and Drozdenko, Daria and
Kawamura, Yoshihito},
title = {{I}n situ diffraction study on the annealing performance of
a rapidly solidified ribbon consolidated
{M}g-{C}a-{Y}-{Z}n-{M}n alloy},
journal = {Journal of magnesium and alloys},
volume = {13},
number = {4},
issn = {2213-9567},
address = {Amsterdam [u.a.]},
publisher = {Elsevier},
reportid = {PUBDB-2025-04066},
pages = {1771 - 1783},
year = {2025},
abstract = {Dilute Mg alloys processed by the rapidly solidified ribbon
consolidation (RSRC) technique are candidate materials for
structural applications due to their enhanced mechanical
performance. The thermal stability of the structure in these
alloys strongly influences their mechanical performance at
elevated temperatures. In this study, an RSRC-processed
$Mg–1\%$ $Ca–0.5\%$ $Zn–0.1\%$ $Y–0.03\%$ Mn
$(at\%)$ alloy was heated at a constant rate up to 833 K,
and concurrently in situ X-ray diffraction (XRD)
measurements were performed using synchrotron radiation in
order to monitor the changes in the structure. In addition,
ex situ electron microscopy investigations were carried out
before and after annealing to complete the XRD study. On the
basis of XRD results, the stages of the microstructure
evolution during heating were identified. In addition, the
thermal expansion coefficients of the matrix and the
Mg$_2$Ca secondary phase were determined. Between 299 and
400 K, the lattice constants of both the matrix and the
Mg$_2$Ca phase increased due to thermal expansion. In the
temperature range of 400-673 K, the increase of the lattice
constants with increasing the temperature continued, but
their rate was different for the two phases which can induce
thermal stresses. Between 673 and 753 K, the lattice
constants of the secondary phase did not change most
probably due to the compensating effects of the thermal
expansion and the decrease of the Ca content. In the
temperature range of 753–793 K, the Mg$_2$Ca phase started
to dissolve. Between 793 and 833 K the dissolution
continued, and additionally the matrix was partially
melted.},
cin = {DOOR ; HAS-User / FS-PETRA-D},
ddc = {540},
cid = {I:(DE-H253)HAS-User-20120731 /
I:(DE-H253)FS-PETRA-D-20210408},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / 6G3 - PETRA III (DESY) (POF4-6G3)},
pid = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G3},
experiment = {EXP:(DE-H253)P-P21.2-20150101},
typ = {PUB:(DE-HGF)16},
doi = {10.1016/j.jma.2025.02.024},
url = {https://bib-pubdb1.desy.de/record/638438},
}