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@ARTICLE{Gubicza:638438,
author = {Gubicza, Jeno and Mathis, Kristian and Nagy, Peter and
Jenei, Péter and Hegedues, Zoltan and Farkas, Andrea and
Veselý, Jozef and Inoue, Shin-ichi and Drozdenko, Daria and
Kawamura, Yoshihito},
title = {{I}n situ diffraction study on the annealing performance of
a rapidly solidified ribbon consolidated
{M}g-{C}a-{Y}-{Z}n-{M}n alloy},
journal = {Journal of magnesium and alloys},
volume = {13},
number = {4},
issn = {2213-9567},
address = {Amsterdam [u.a.]},
publisher = {Elsevier},
reportid = {PUBDB-2025-04066},
pages = {1771 - 1783},
year = {2025},
note = {Open access},
abstract = {Dilute Mg alloys processed by the rapidly solidified ribbon
consolidation (RSRC) technique are candidate materials for
structural applications due to their enhanced mechanical
performance. The thermal stability of the structure in these
alloys strongly influences their mechanical performance at
elevated temperatures. In this study, an RSRC-processed
$Mg–1\%$ $Ca–0.5\%$ $Zn–0.1\%$ $Y–0.03\%$ Mn
$(at\%)$ alloy was heated at a constant rate up to 833 K,
and concurrently in situ X-ray diffraction (XRD)
measurements were performed using synchrotron radiation in
order to monitor the changes in the structure. In addition,
ex situ electron microscopy investigations were carried out
before and after annealing to complete the XRD study. On the
basis of XRD results, the stages of the microstructure
evolution during heating were identified. In addition, the
thermal expansion coefficients of the matrix and the Mg2Ca
secondary phase were determined. Between 299 and 400 K, the
lattice constants of both the matrix and the Mg2Ca phase
increased due to thermal expansion. In the temperature range
of 400-673 K, the increase of the lattice constants with
increasing the temperature continued, but their rate was
different for the two phases which can induce thermal
stresses. Between 673 and 753 K, the lattice constants of
the secondary phase did not change most probably due to the
compensating effects of the thermal expansion and the
decrease of the Ca content. In the temperature range of
753–793 K, the Mg2Ca phase started to dissolve. Between
793 and 833 K the dissolution continued, and additionally
the matrix was partially melted.},
cin = {DOOR ; HAS-User / FS-PETRA-D},
ddc = {540},
cid = {I:(DE-H253)HAS-User-20120731 /
I:(DE-H253)FS-PETRA-D-20210408},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / 6G3 - PETRA III (DESY) (POF4-6G3)},
pid = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G3},
experiment = {EXP:(DE-H253)P-P21.2-20150101},
typ = {PUB:(DE-HGF)16},
doi = {10.1016/j.jma.2025.02.024},
url = {https://bib-pubdb1.desy.de/record/638438},
}