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@ARTICLE{Constantinou:638190,
author = {Constantinou, Anna P. and Zheng, Feifei and Wang, Lezhi and
Xu, Wenqi and Li, Qian and Zhan, Beini and Salvado Correia,
Joana and SomuncuoĞlu, Birsen and Da Vela, Stefano and
Papadakis, Christine M. and Georgiou, Theoni K.},
title = {{T}hermogels {B}ased on {B}lock versus {G}radient
{T}erpolymers: {D}ifferences in the {N}ano- and
{M}acro-{S}cale},
journal = {Macromolecules},
volume = {58},
number = {17},
issn = {0024-9297},
address = {Washington, DC},
publisher = {Soc.},
reportid = {PUBDB-2025-04008},
pages = {9122 - 9139},
year = {2025},
abstract = {In the present study, the effect of the distribution of
repeated units in copolymers based on oligo(ethylene glycol)
methyl ether methacrylate (A), n-butyl methacrylate (B), and
di(ethylene glycol) methyl ether methacrylate (C) is
reported and discussed for the first time. Several linear
structures have been synthesized via group transfer
polymerization, varying from statistical to gradient to
block structures. Notably, among the other linear
architectures, we report the one-pot synthesis of a forced
gradient terpolymer and the investigation of its
thermoresponsive and gelation properties. It is proven that
the distribution of repeated units along the polymer chain
governs the solubility and gelation of the copolymers, with
the ABC and gradient structures being the best-performing.
The self-assembled structures and aggregation mechanisms
differ strongly for the ABC triblock and the gradient
terpolymer, as revealed by synchrotron small-angle X-ray
scattering. The promising results of the gradient structure
open a new era for designing novel copolymers with potential
applications in the biomedical sector.},
cin = {EMBL-User / EMBL},
ddc = {540},
cid = {I:(DE-H253)EMBL-User-20120814 / I:(DE-H253)EMBL-20120731},
pnm = {6G3 - PETRA III (DESY) (POF4-6G3)},
pid = {G:(DE-HGF)POF4-6G3},
experiment = {EXP:(DE-H253)P-P12-20150101},
typ = {PUB:(DE-HGF)16},
doi = {10.1021/acs.macromol.5c00821},
url = {https://bib-pubdb1.desy.de/record/638190},
}