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@ARTICLE{Choong:638016,
author = {Choong, Choe Earn and Hong, YuKyung and Nandy, Subhajit and
Wong, Kien Tiek and Weng, Bo and Choi, Eunjin and Yoon,
Yeomin and Jang, Min},
title = {{M}icro-environment regulation for strong metal–support
interaction in ${R}u{O}_2$-doped barium cerate for boosting
photocatalytic ammonia production},
journal = {Applied catalysis / B},
volume = {382},
issn = {0926-3373},
address = {Amsterdam},
publisher = {Elsevier},
reportid = {PUBDB-2025-03964},
pages = {125870},
year = {2026},
note = {These measurements were carried out during in house
research beamtime: H-20010499 Waiting for fulltext},
abstract = {Modulating the local microenvironment via strong
metal-support interaction (SMSI) approach in Ru-based
photocatalyst for improving photocatalytic ammonia
production is poorly understood. Herein, we investigate the
mechanism of the SMSI effect of RuO$_2$ on barium cerate
(BC) by forming Ru-O-Ce electron transfer channel to enhance
the photocatalytic ammonium (NH$_4^+$) production. Among the
prepared photocatalysts, BC-Ru$_{0.25}$ showed the highest
NH$_4^+$ formation rate of 3.533 mmol g$^{−1}$
h$^{−1}$ with a 5.464 \% apparent quantum efficiency
(AQE), which was 5.17-fold higher than BC. In-situ X-ray
photoelectron spectroscopy (XPS) and X-ray absorption near
edge structure (XANES) analyses revealed that RuO$_2$ doping
on BC promoted the formation of Ru-O-Ce bonds and degenerate
barium 3d orbitals, creating an asymmetric coordination
environment that improved N$_2$ interaction. Additionally,
the formation of a Ru-O-Ce electron channel on BC prolonged
the electron decay time and improved spatial separation,
resulting in higher nitric oxide (NO) radical formation due
to the promotion of hydroxyl radical generation from
photoexcited holes. Notably, in-situ surface-enhanced Raman
spectroscopy (SERS) analysis revealed that RuO$_2$ loading
on BC altered the electronic state of Ba owing to the SMSI
effect, improved N$_2$ interaction on the Ba-O bonds, and
facilitated the NH$_4^+$ production. Density functional
theory (DFT) calculations showed that RuO$_2$-doping of BC
can result in Ba-N bonding and promote the nitric oxide
reduction reaction (NORR) by reducing the energy barrier of
the rate-determining step and accelerating the protonation
process. This study demonstrates the SMSI effects via the
strategy of a Ru-based dopant on NH$_4^+$ photocatalytic
production.},
cin = {FS-PETRA-S / DOOR ; HAS-User},
ddc = {540},
cid = {I:(DE-H253)FS-PETRA-S-20210408 /
I:(DE-H253)HAS-User-20120731},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / 6G3 - PETRA III (DESY) (POF4-6G3)},
pid = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G3},
experiment = {EXP:(DE-H253)P-P64-20150101},
typ = {PUB:(DE-HGF)16},
doi = {10.1016/j.apcatb.2025.125870},
url = {https://bib-pubdb1.desy.de/record/638016},
}