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@ARTICLE{Yang:637980,
author = {Yang, Ye and Wu, Yufeng and Liu, Chang and Hambsch, Mike
and Dong, Tiange and Bodesheim, David and Prasad, Mahabir
and Dianat, Arezoo and Kühne, Thomas D. and Cuniberti,
Gianaurelio and Mannsfeld, Stefan and Parkin, Stuart S. P.
and Dong, Renhao and Wang, Zhiyong and Feng, Xinliang},
title = {{O}n-liquid surface synthesis of diyne-linked
two-dimensional polymer crystals},
journal = {Nature Communications},
volume = {16},
number = {1},
issn = {2041-1723},
address = {[London]},
publisher = {Springer Nature},
reportid = {PUBDB-2025-03949},
pages = {8243},
year = {2025},
abstract = {The synthesis of thin crystalline two-dimensional polymers
(2DPs) typically relies on reversible dynamic covalent
reactions. While substantial progress has been made in
solution-based and interfacial syntheses, achieving 2DPs
through irreversible carbon-carbon coupling reactions
remains a formidable challenge. Herein, we present an
on-liquid surface (a mixture of N,N-dimethylacetamide and
water, DMAc-H$_2$O) synthesis method for constructing
diyne-linked 2DP (DY$_2$DP) crystals via Glaser coupling,
assisted by a perfluoro-surfactant (PFS) monolayer. In-situ
spectroscopic and diffraction techniques reveal that the
well-ordered PFS monolayer facilitates the accumulation of
Cu$^+$ ions and subsequent vertical coupling of acetylenic
monomers on the DMAc-H$_2$O surface. Building on these
findings, we successfully synthesized micro-scale rod-shaped
DY$_2$DP-Por or graphdiyne (GDY) crystals through the
polymerization of porphyrin- or benzene-based monomers,
respectively. Our study represents a significant advancement
in the field of on-liquid surface chemistry and opens up
enormous opportunities for constructing C—C bond linked
2DP crystals with unique functionalities.},
cin = {FS DOOR-User},
ddc = {500},
cid = {$I:(DE-H253)FS_DOOR-User-20241023$},
pnm = {6G3 - PETRA III (DESY) (POF4-6G3) / FS-Proposal: I-20230315
(I-20230315) / FS-Proposal: I-20230364 (I-20230364) /
FC2DMOF - Development of Functional Conjugated
Two-Dimensional Metal-Organic Frameworks (852909) / T2DCP -
Development of Thiophene Based Conjugated Polymers in Two
Dimensions (819698) / DFG project G:(GEPRIS)426572620 -
Synthese von kristallinen, supramolekularen
Polyanilinschichten/2D-Polyanilinen und deren
Strukturbestimmung mittels Elektronenbeugung und
TEM-Bildgebung (426572620) / GRK 2861 - GRK 2861: Planare
Kohlenstoffgitter (491865171) / DFG project
G:(GEPRIS)417590517 - SFB 1415: Chemie der synthetischen
zweidimensionalen Materialien (417590517)},
pid = {G:(DE-HGF)POF4-6G3 / G:(DE-H253)I-20230315 /
G:(DE-H253)I-20230364 / G:(EU-Grant)852909 /
G:(EU-Grant)819698 / G:(GEPRIS)426572620 /
G:(GEPRIS)491865171 / G:(GEPRIS)417590517},
experiment = {EXP:(DE-H253)P-P08-20150101},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:40921732},
doi = {10.1038/s41467-025-63768-6},
url = {https://bib-pubdb1.desy.de/record/637980},
}