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@ARTICLE{Davoodi:637649,
author = {Davoodi, Saeed and Namata, Faridah and Rosén, Tomas and
Roth, Stephan V. and Malkoch, Michael and Söderberg, L.
Daniel and Lundell, Fredrik},
title = {{T}uning {A}lignment, {S}trength, and {T}oughness in
{F}unctional {C}ellulose:{H}elux {F}ilaments: {A}
{M}olecular {T}rade-{O}ff},
journal = {Biomacromolecules},
volume = {26},
number = {7},
issn = {1525-7797},
address = {Columbus, Ohio},
publisher = {American Chemical Soc.},
reportid = {PUBDB-2025-03875},
pages = {4133 - 4145},
year = {2025},
abstract = {The complex architecture of wood motivates studies of
bioinspired materials that combine strength, toughness, and
mechanical integrity. We explore the interplay between
nanofiber alignment and molecular interactions in composite
filaments formed from cellulose nanofibers (CNFs) and a
dendritic polyampholyte, Helux. Helux enhances strength by
$60\%$ and increases toughness 5-fold through ionic bonding
and thermal covalent cross-linking. However, wide-angle
X-ray scattering (WAXS) reveals reduced nanofiber alignment
in Helux-containing samples, resulting in a $25\%$ decrease
in stiffness─highlighting a trade-off between structural
order and cohesion. Polarized optical microscopy (POM) and
in situ small-angle X-ray scattering (SAXS) attribute this
reduced alignment to enhanced rotary diffusion, driven by
carboxylate groups of the Helux. With Helux, multivalent
links across the nanofibers give a denser and tougher
network with fewer voids. This behavior resembles lignin and
hemicellulose interactions in wood, where flexibility and
cohesion govern the performance.},
cin = {DOOR ; HAS-User / FS-SMA},
ddc = {570},
cid = {I:(DE-H253)HAS-User-20120731 / I:(DE-H253)FS-SMA-20220811},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / 6G3 - PETRA III (DESY) (POF4-6G3) /
SWEDEN-DESY - SWEDEN-DESY Collaboration
$(2020_Join2-SWEDEN-DESY)$ / FS-Proposal: I-20220555 EC
(I-20220555-EC)},
pid = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G3 /
$G:(DE-HGF)2020_Join2-SWEDEN-DESY$ /
G:(DE-H253)I-20220555-EC},
experiment = {EXP:(DE-H253)P-P03-20150101},
typ = {PUB:(DE-HGF)16},
doi = {10.1021/acs.biomac.5c00128},
url = {https://bib-pubdb1.desy.de/record/637649},
}