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@ARTICLE{Lehmkhler:637202,
      author       = {Lehmkühler, Felix and Westermeier, Fabian and
                      Barrios-Capuchino, Juan J. and Weschke, Daniel and Dallari,
                      Francesco and Roseker, Wojciech and Parak, Wolfgang J. and
                      Schulz, Florian},
      title        = {{M}onitoring nanoparticle self-assembly on liquid subphases
                      in situ in a vertical scattering geometry},
      journal      = {Nano trends},
      volume       = {11},
      issn         = {2666-9781},
      address      = {[Amsterdam]},
      publisher    = {Elsevier},
      reportid     = {PUBDB-2025-03811},
      pages        = {100132},
      year         = {2025},
      abstract     = {Nanoparticle (NP) self-assembly is a promising tool for the
                      straightforward preparation of complex materials without
                      lithography. Self-assembly on liquid subphases is
                      established for the preparation of thin NP films with
                      quasicrystalline order on large scales. Small-angle X-ray
                      scattering (SAXS) at synchrotron radiation sources is in
                      particular advantageous to study self-assembly in situ,
                      providing detailed structural information with high temporal
                      resolution. Here we present a new experimental setup that
                      allows measuring SAXS in a vertical geometry. This way it is
                      possible to study the self-assembly of nanoparticles on
                      liquid subphases in situ as demonstrated with gold
                      nanoparticles. In contrast to measurements with grazing
                      incidence (GISAXS), spatial resolution in the µm range and
                      sampling of the volume material is possible. Integration of
                      optical microscopy allows observing the measurement position
                      and formation of supercrystal flakes. The setup can be used
                      to study self-assembly of various nanoparticles on liquid
                      subphases but is not limited to such studies. It was
                      realized at the beamline P10 at PETRA III (Deutsches
                      Elektronen-Synchrotron DESY, Hamburg, Germany).},
      cin          = {DOOR ; HAS-User / FS-SMP / FS-PETRA-S},
      ddc          = {530},
      cid          = {I:(DE-H253)HAS-User-20120731 / I:(DE-H253)FS-SMP-20171124 /
                      I:(DE-H253)FS-PETRA-S-20210408},
      pnm          = {632 - Materials – Quantum, Complex and Functional
                      Materials (POF4-632) / 6G3 - PETRA III (DESY) (POF4-6G3) /
                      AIM, DFG project G:(GEPRIS)390715994 - EXC 2056: CUI:
                      Advanced Imaging of Matter (390715994) / REScala - A
                      Programming Platform for Reactive Data-intensive
                      Applications (862535) / FS-Proposal: I-20211357 (I-20211357)
                      / FS-Proposal: I-20221388 (I-20221388)},
      pid          = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G3 /
                      G:(GEPRIS)390715994 / G:(EU-Grant)862535 /
                      G:(DE-H253)I-20211357 / G:(DE-H253)I-20221388},
      experiment   = {EXP:(DE-H253)P-P10-20150101},
      typ          = {PUB:(DE-HGF)16},
      doi          = {10.1016/j.nwnano.2025.100132},
      url          = {https://bib-pubdb1.desy.de/record/637202},
}