%0 Journal Article %A Wang, Wei %A Yu, Zhipeng %A Yue, Liguo %A Çaha, Ihsan %A Zhang, Weicai %A Chen, Qingqing %A Huang, Haoliang %A Lin, Fei %A Zhao, Yang %A Zeng, Jinfeng %A Lu, Jingcheng %A Deepak, Francis Leonard %A Liu, Lifeng %T Regulating Electronic Structure and Coordination Environment of Transition Metal Selenides through the High-Entropy Strategy for Expedited Lithium–Sulfur Chemistry %J ACS nano %V 19 %N 30 %@ 1936-0851 %C Washington, DC %I Soc. %M PUBDB-2025-03725 %P 27440 - 27454 %D 2025 %X Transition metal diselenides (TMSe<sub>2</sub>) have proven as promising catalysts able to promote the conversion kinetics of lithium polysulfides (LiPSs) in lithium–sulfur batteries (LSBs). However, the limited number of catalytically active edge sites in TMSe<sub>2</sub> severely hinders the realization of their full potential for boosting LSB’s performance. Herein, we report the synthesis of high-entropy NiCoMnCrVSe<sub>2</sub> nanoflakes anchored on graphene supports (NiCoMnCrVSe<sub>2</sub>/G) through a microwave-assisted solvothermal method. We systematically investigate how the high-entropy strategy enables the regulation of the electronic structure and coordination of various metal species in TMSe<sub>2</sub> through comprehensive experimental studies and theoretical calculations. Our results show that as the number of transition metals in TMSe<sub>2</sub> increases, the d-band center of metal active sites upshifts toward the Fermi level and the difference among d-band centers of various metal species diminishes, which facilitates the adsorption of LiPSs and lowers the energy barriers to nucleation/decomposition of Li<sub>2</sub>S. Consequently, LSBs containing NiCoMnCrVSe<sub>2</sub>/G as sulfur hosts deliver a high specific discharge capacity of 1453 mAh g<sup>–1</sup> at 0.1 C and excellent stability at 1 C for 500 cycles with a low decay rate of merely 0.016 %F PUB:(DE-HGF)16 %9 Journal Article %R 10.1021/acsnano.5c05720 %U https://bib-pubdb1.desy.de/record/636994