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@ARTICLE{Antil:636254,
author = {Antil, Neha and Louis Anandaraj, Savarithai Jenani and
Kang, Liqun and Ghazi Zahedi, Hooman and DeBeer, Serena and
Leitner, Walter and Bordet, Alexis},
title = {{R}uthenium {N}anoparticles on {W}ater-{S}table {S}upported
{I}onic {L}iquid {P}hases as {C}atalytic {S}ystems for
{A}queous {P}hase {CO}$_2$ {H}ydrogenation},
journal = {ACS catalysis},
volume = {15},
issn = {2155-5435},
address = {Washington, DC},
publisher = {ACS},
reportid = {PUBDB-2025-03636},
pages = {14601 - 14610},
year = {2025},
abstract = {The first example of a hydrothermally stable Supported
Ionic Liquid Phase (SILP) material was designed and used
successfully as a support for ruthenium nanoparticles (Ru
NPs) in catalytic hydrogenation of CO$_2$ to formic acid in
water/amine media. Imidazolium-based ionic liquids (ILs)
were grafted on activated carbon (AC) through the formation
of robust carbon–carbon bonds via diazotization, followed
by deposition of Ru NPs using an organometallic approach.
Compared to reference materials, the presence of the IL on
the solid material led not only to improved catalyst
performance of the nanoparticles but also to higher formic
acid concentrations in the reaction mixture due to
additional thermodynamic stabilization of the product. The
Ru@SILPAC catalysts showed high activity (turnover
frequencies (TOFs) exceeding 3000 h$^{–1}$), productivity
(turnover numbers (TONs) up to 15,000 in a single batch),
and stability (10 recycling with no apparent loss of
activity). These results define a new benchmark for NP-based
catalysts in CO2 hydrogenation to formic acid and suggest
promising potential for the application of such NP@SILP
materials in aqueous phase hydrogenation reactions in
general.},
cin = {FS DOOR-User},
ddc = {540},
cid = {$I:(DE-H253)FS_DOOR-User-20241023$},
pnm = {6G3 - PETRA III (DESY) (POF4-6G3) / FS-Proposal: I-20230324
(I-20230324) / DFG project G:(GEPRIS)390919832 - EXC 2186:
Das Fuel Science Center – Adaptive Umwandlungssysteme für
erneuerbare Energie- und Kohlenstoffquellen (390919832)},
pid = {G:(DE-HGF)POF4-6G3 / G:(DE-H253)I-20230324 /
G:(GEPRIS)390919832},
experiment = {EXP:(DE-H253)P-P65-20150101},
typ = {PUB:(DE-HGF)16},
doi = {10.1021/acscatal.5c03605},
url = {https://bib-pubdb1.desy.de/record/636254},
}