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@ARTICLE{An:633262,
author = {An, Siyu and Sahu, Rajib and Zhang, Ruizhuo and Ulusoy,
Fatih and Kübel, Christian and Kondrakov, Aleksandr and
Janek, Juergen and Brezesinski, Torsten},
title = {{T}itanium {S}ubstitution to {A}dvance the {P}rospect of
{N}a{M}n{O}$_2$ {C}athodes for {P}ractical {A}pplication in
{S}odium-{I}on {B}atteries},
journal = {ACS applied energy materials},
volume = {8},
number = {14},
issn = {2574-0962},
address = {Washington, DC},
publisher = {ACS Publications},
reportid = {PUBDB-2025-02388},
pages = {10508 - 10518},
year = {2025},
abstract = {O3-type layered oxides stand out among various Na-ion
battery cathodes due to their unparalleled theoretical
specific capacities. As a representative of low-cost,
Mn-based cathode materials, $α$-NaMnO$_2$ (NMO) has
attracted great attention. However, its practical
application is hindered by poor reversibility. Compared to
other O3 or O′3-type layered oxides, such as NaNiO2, NMO
undergoes multiple phase transitions, with the final O1
phase negatively affecting cycling performance. In this
study, precipitated Mn$_3$O$_4$ was employed, to our
knowledge for the first time, as a precursor in the
synthesis of NMO, and the cathode material was
systematically optimized through incremental improvement via
titanium substitution. NaMn$_{0.9}$Ti$_{0.1}$O$_2$ was found
to exhibit enhanced stability, with the capacity retention
increasing from 42 to 70\% after 50 cycles at C/10, along
with superior rate capability over NMO. This is due in part
to titanium’s role in facilitating primary particle
(grain) growth and suppressing O1 phase formation, thereby
preserving structural integrity and mitigating degradation
caused by volume variations and irreversible oxygen redox
during battery operation. This work not only provides
valuable insights into the development of next-generation
NMO cathodes but also advances their potential for practical
applications.},
cin = {DOOR ; HAS-User},
ddc = {540},
cid = {I:(DE-H253)HAS-User-20120731},
pnm = {6G3 - PETRA III (DESY) (POF4-6G3) / FS-Proposal: I-20230867
(I-20230867)},
pid = {G:(DE-HGF)POF4-6G3 / G:(DE-H253)I-20230867},
experiment = {EXP:(DE-H253)P-P02.1-20150101},
typ = {PUB:(DE-HGF)16},
doi = {10.1021/acsaem.5c01367},
url = {https://bib-pubdb1.desy.de/record/633262},
}