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@ARTICLE{Lin:633261,
author = {Lin, Jing and Schaller, Mareen and Zhang, Ruizhuo and
Baran, Volodymyr and Liu, Hao and Ding, Ziming and Indris,
Sylvio and Kondrakov, Aleksandr and Brezesinski, Torsten and
Strauss, Florian},
title = {{H}igh-entropy argyrodite glass–ceramic electrolytes for
all-solid-state batteries},
journal = {Materials futures},
volume = {4},
number = {2},
issn = {2752-5724},
address = {Bristol},
publisher = {IOP Science},
reportid = {PUBDB-2025-02387},
pages = {025105},
year = {2025},
abstract = {Lithium argyrodite superionic conductors with the general
formula Li$_6$PS$_5$X (X = Cl, Br, I) have been intensively
investigated in recent years and successfully adopted in the
field of solid-state batteries (SSBs). The transport
properties of argyrodite solid electrolytes (SEs) usually
strongly depend on the degree of occupational disorder.
Increasing disorder through complex doping or substitution
has been shown to directly affect ionic conductivity.
Herein, we explore a high-entropy lithium argyrodite of
nominal composition
Li$_{6.6}$[P$_{0.2}$Si$_{0.2}$Sn$_{0.2}$Ge$_{0.2}$Sb$_{0.2}$]S$_5$I.
This material can be readily prepared by mechanochemistry.
Using complementary diffraction techniques, nuclear magnetic
resonance spectroscopy, and charge-transport measurements,
we show that upon tailoring crystallinity and defect
concentration by post-annealing at temperatures up to 220
°C, a high room-temperature ionic conductivity of about 0.9
mS cm$^{−1}$ (∼4.4 mS cm$^{−1}$ bulk conductivity) can
be achieved. Both the as-prepared and annealed (at 220 °C)
samples were tested in pellet-stack SSB cells. The
mechanochemically prepared glass–ceramic SE was found to
exhibit superior performance, even outperforming
commercially available Li$_6$PS$_5$Cl. Collectively, the
results highlight the importance of considering structural
aspects across different length scales when optimizing the
properties of lithium argyrodites for SSB applications.},
cin = {DOOR ; HAS-User / FS-PET-D},
ddc = {600},
cid = {I:(DE-H253)HAS-User-20120731 /
I:(DE-H253)FS-PET-D-20190712},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / 6G3 - PETRA III (DESY) (POF4-6G3)},
pid = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G3},
experiment = {EXP:(DE-H253)P-P02.1-20150101},
typ = {PUB:(DE-HGF)16},
doi = {10.1088/2752-5724/adde76},
url = {https://bib-pubdb1.desy.de/record/633261},
}