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000632812 0247_ $$2ISSN$$a1600-8596
000632812 0247_ $$2ISSN$$a2053-2733
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000632812 1001_ $$0P:(DE-H253)PIP1089491$$aLi, Chufeng$$b0$$eCorresponding author$$udesy
000632812 1112_ $$aTwenty-Sixth Congress and General Assembly of the International Union of Crystallography$$cMelbourne$$d2023-08-22 - 2023-08-29$$gIUCr 2023$$wAustralia
000632812 245__ $$aConvergent beam X-ray crystallography and 3D diffraction imaging using multilayer Laue lenses
000632812 260__ $$c2023
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000632812 520__ $$acrystallography and 3D diffraction microscopy. Our recent MLLs achieve a numerical aperture (NA) of ~ 0.02 at a photon energy of 17.5 keV (or 0.71 Å wavelength), meaning that beam converges onto the focus over an angular range of 40 mrad or 1.3º. When the crystal is placed downstream of the focus, there is a correlation between position in the beam and the angle of incidence of a ray. The crystal selects Bragg reflections from the supplied range of angles, at particular locations of the crystal (slices, in the case of a single crystal). In this configuration, the diffraction data provides a mix of crystallography and (tomographic) microscopy. We are particularly interested in developing convergent-beam diffraction as a way to obtain fully-integrated Bragg reflections in single exposures (to reduce the number of patterns required in serial crystallography at free-electron laser sources) and to obtain structure factors of high accuracy by observing and accounting for spatial variations in crystals, such as their shape, strain, or defect structure. Additionally, using the mapping between position and incidence angle, 3-D microscopic images of the diffraction efficiency of the crystal was obtained from the same data set. The simple experimental setup and data collection strategy offers advantages such as ample operational space and easy adjustment of the spatial resolution by changing the geometry. The convergent beam diffraction (CBD) scheme, with further development in progress is potentially applicable to multi-scale structural or dynamics studies for both material and life sciences.
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000632812 7001_ $$0P:(DE-H253)PIP1086928$$aIvanov, Nikolay$$b1
000632812 7001_ $$0P:(DE-H253)PIP1016171$$aPrasciolu, Mauro$$b2
000632812 7001_ $$0P:(DE-H253)PIP1011659$$aFleckenstein, Holger$$b3
000632812 7001_ $$0P:(DE-H253)PIP1020481$$aDomaracky, Martin$$b4
000632812 7001_ $$0P:(DE-H253)PIP1088012$$aDresselhaus, J. Lukas$$b5
000632812 7001_ $$0P:(DE-H253)PIP1006155$$aYefanov, Oleksandr$$b6
000632812 7001_ $$0P:(DE-H253)PIP1097799$$aZhang, Wenhui$$b7
000632812 7001_ $$0P:(DE-H253)PIP1100352$$aZakharova, Margarita$$b8
000632812 7001_ $$0P:(DE-H253)PIP1006208$$aMeents, Alke$$b9
000632812 7001_ $$0P:(DE-H253)PIP1005088$$aDelmas, Tjark$$b10
000632812 7001_ $$0P:(DE-H253)PIP1101040$$aDe Gennaro Aquino, Ivan$$b11
000632812 7001_ $$0P:(DE-H253)PIP1012087$$aOberthuer, Dominik$$b12
000632812 7001_ $$0P:(DE-H253)PIP1015903$$aSprenger, Janina$$b13
000632812 7001_ $$0P:(DE-H253)PIP1099331$$aPateras, Anastasios$$b14
000632812 7001_ $$0P:(DE-H253)PIP1084014$$aHenkel, Alessandra$$b15
000632812 7001_ $$0P:(DE-HGF)0$$aMashhour, Aida Rahmani$$b16
000632812 7001_ $$0P:(DE-H253)PIP1013442$$aHakanpää, Johanna$$b17
000632812 7001_ $$0P:(DE-H253)PIP1006443$$aBajt, Saša$$b18
000632812 7001_ $$0P:(DE-H253)PIP1006324$$aChapman, Henry N.$$b19
000632812 773__ $$0PERI:(DE-600)2020844-3$$a10.1107/S2053273323092495$$gVol. 79, no. a2, p. C366 - C366$$x2053-2733$$y2023
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