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@ARTICLE{Tober:631049,
author = {Tober, Steffen and Schober, Jan-Christian and Creutzburg,
Marcus and Beck, Esko Erik and Semione, Guilherme Dalla Lana
and Chung, Simon and Jacobse, Leon and Arndt, Bjoern and
Vlad, Alina and Steinbrügge, René and Wille,
Hans-Christian and Sergeev, Ilya and Noei, Heshmat and
Schlage, Kai and Leupold, Olaf and Vonk, Vedran and Stierle,
Andreas},
title = {{S}ite-{R}esolved {N}ear-{S}urface {C}ation {D}iffusion in
{M}agnetite},
journal = {Physical review letters},
volume = {134},
number = {23},
issn = {0031-9007},
address = {College Park, Md.},
publisher = {APS},
reportid = {PUBDB-2025-01918},
pages = {236203},
year = {2025},
abstract = {In situ nuclear forward scattering shows a thermally
induced cation exchange between a 57 Fe3 O4 thin-film and
a Fe3 O4 (001) substrate predominantly in the octahedral
sublattice for a temperature range between 470 and 710 K.
The overall activation barrier in this temperature range is
found to be 19±32 kJ/mol, which is significantly lower
than expected from extrapolating a bulk diffusion model.
This observation can be attributed to the large
out-of-equilibrium cation deficit as determined by surface
x-ray diffraction. Despite the relatively low hopping
barrier, the diffusion constant is about 5 orders of
magnitude lower than expected for magnetite having an
equilibrium cation stoichiometry. The results are relevant
for applications relying on the near-surface structure and
stoichiometry of magnetite, and we argue that the
correlation between cation diffusion and stoichiometry may
play a role for a wider range of oxide materials.},
cin = {FS-NL / FS-PETRA-S},
ddc = {530},
cid = {I:(DE-H253)FS-NL-20120731 / I:(DE-H253)FS-PETRA-S-20210408},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / SFB 986 C07 - Deposition und
Stabilität von hochtemperaturfesten geschichteten
Metamaterialien (C07) (318029273) / DFG project
G:(GEPRIS)192346071 - SFB 986: Maßgeschneiderte
Multiskalige Materialsysteme - M3 (192346071)},
pid = {G:(DE-HGF)POF4-632 / G:(GEPRIS)318029273 /
G:(GEPRIS)192346071},
experiment = {EXP:(DE-H253)Nanolab-01-20150101 /
EXP:(DE-H253)Nanolab-02-20150101 /
EXP:(DE-H253)Nanolab-03-20150101 /
EXP:(DE-H253)P-P01-20150101},
typ = {PUB:(DE-HGF)16},
doi = {10.1103/PhysRevLett.134.236203},
url = {https://bib-pubdb1.desy.de/record/631049},
}