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@ARTICLE{Bittinger:630145,
author = {Bittinger, Sophia C. and Struck, Jana and Dobschall, Finn
and Benthien, Sophie and Hartmann, Hauke and Schlicke,
Hendrik and Kohantorabi, Mona and Noei, Heshmat and
Vossmeyer, Tobias},
title = {{N}anocomposites of {T}itania/{R}educed {G}raphene {O}xide:
{F}lexible {H}umidity {S}ensors {T}uned via {P}hotocatalytic
{R}eduction},
journal = {ACS applied nano materials},
volume = {8},
number = {15},
issn = {2574-0970},
address = {Washington, DC},
publisher = {ACS Publications},
reportid = {PUBDB-2025-01850},
pages = {7428 - 7439},
year = {2025},
abstract = {In this study, we demonstrate the tunability of hybrid
graphene oxide/reduced graphene oxide/titania nanocrystal
(GO/rGO/TNC) films for resistive humidity sensing through
photocatalytic reduction. Using a layer-by-layer
spin-coating (LbL-SC) technique, we fabricate GO/TNC
nanofilms with titania nanorods (TNRs) or nanoplates (TNPs)
on various substrates, achieving high uniformity and precise
control over the film thickness (15–150 nm). We
investigate the evolution of the electrical, optical, and
structural properties of these films, modulated by the
photocatalytic activity of TNCs under UV exposure (254 nm)
while varying the illumination time, TNC type, and film
thickness. The inclusion of TNCs enhances the films’
conductivity by several orders of magnitude compared to pure
GO films under UV illumination and enables precise
adjustment of the GO/rGO and (GO/rGO)/TNC ratios. This
approach is used for tuning the sensitivity, response time,
and response polarity of (GO/rGO)/TNC resistors on flexible
substrates to changes in relative humidity (RH). TNP-based
films demonstrate superior performance, achieving
sensitivities of up to 2.2 and response times as short as 1
s over a broad range of RH levels (∼35 to $85\%$ and ∼1
to $80\%).$ Depending on the composition and RH level, the
sensors exhibit both positive and negative resistive
responses to increasing humidity. Gravimetric analyses show
that films with varying GO/rGO ratios exhibit the same
change in water mass uptake, indicating that the differences
in resistive behavior are driven by UV-induced alterations
in their chemical and electrical properties. Finally, we
propose the use of these sensors to detect body-related
humidity fluctuations, demonstrating their suitability for
wearable electronics. Our results highlight the potential
applicability of (GO/rGO)/TNC nanocomposites as highly
customizable humidity sensors.},
cin = {FS-NL},
ddc = {540},
cid = {I:(DE-H253)FS-NL-20120731},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / DFG project G:(GEPRIS)395896547 -
Multifunktionale Membranen aus Graphenoxid und
TiO2-Nanokristallen: Steuerung elektrischer, mechanischer
und elektromechanischer Eigenschaften durch
photokatalytische Reduktion (395896547)},
pid = {G:(DE-HGF)POF4-632 / G:(GEPRIS)395896547},
experiment = {EXP:(DE-H253)Nanolab-02-20150101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:001461018600001},
doi = {10.1021/acsanm.4c06524},
url = {https://bib-pubdb1.desy.de/record/630145},
}