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@ARTICLE{DalMolin:627891,
author = {Dal Molin, Emiliano S. and Javed, Mudassar and Brösigke,
Georg and Rudolph, Maik Alexander and Repke, Jens-Uwe and
Schomäcker, Reinhard and Simon, Ulla and Bekheet, Maged F.
and Gurlo, Aleksander},
title = {{A}dditively {M}anufactured {Z}irconia-{S}upported {I}ndium
{O}xide {C}atalysts and {T}heir {P}erformance in {D}irect
{M}ethanol {S}ynthesis},
journal = {Industrial $\&$ engineering chemistry research},
volume = {64},
number = {2},
issn = {0888-5885},
address = {Columbus, Ohio},
publisher = {American Chemical Society},
reportid = {PUBDB-2025-01666},
pages = {1032 - 1045},
year = {2025},
abstract = {In$_2$O$_3$/ZrO$_2$-based materials are emerging as
candidates for the next generation of industrial catalysts
for direct methanol synthesis. In this research, such
catalysts were additively manufactured into two distinct
geometries that exhibit different pressure drops and
activity profiles, both among themselves and in comparison
to extrudates. The monoliths produced were comprehensively
characterized using a range of techniques, including gas
sorption, X-ray diffraction, micro X-ray fluorescence, and
Raman mapping, to verify their phase and chemical
composition. Computational fluid dynamics was employed to
simulate the gas flow through these structures,
corroborating that the variations in the accessible surface
area are the reason for changes in their performance.
Furthermore, the postreaction characterization provides some
insight into the catalysts’ degradation mechanisms under
hydrogen-rich conditions, identifying the migration of
indium oxide to the catalyst surface and pore blocking as
possible causes of the loss of activity.},
cin = {FS DOOR-User},
ddc = {660},
cid = {$I:(DE-H253)FS_DOOR-User-20241023$},
pnm = {6G3 - PETRA III (DESY) (POF4-6G3) / DFG project
G:(GEPRIS)390540038 - EXC 2008: Unifying Systems in
Catalysis "UniSysCat" (390540038) / FS-Proposal: II-20210010
(II-20210010) / FS-Proposal: I-20220620 (I-20220620)},
pid = {G:(DE-HGF)POF4-6G3 / G:(GEPRIS)390540038 /
G:(DE-H253)II-20210010 / G:(DE-H253)I-20220620},
experiment = {EXP:(DE-H253)P-P02.2-20150101 /
EXP:(DE-H253)P-P64-20150101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:001389937400001},
doi = {10.1021/acs.iecr.4c03439},
url = {https://bib-pubdb1.desy.de/record/627891},
}